N--6-cyclohexyl-2(S)-isopropylhexanoyl>-L-isoleucyl>-2-pyridylmethylamine

Base Information

Chemical Name:N--6-cyclohexyl-2(S)-isopropylhexanoyl>-L-isoleucyl>-2-pyridylmethylamine
CAS No.:132235-90-6
Molecular Formula:C₃₃H₆₀N₄O₃Si
Molecular Weight:588.95
Hs Code.:

N-<N-<5(S)-amino-4(S)-<(tert-butyldimethylsilyl)oxy>-6-cyclohexyl-2(S)-isopropylhexanoyl>-L-isoleucyl>-2-pyridylmethylamine

Synonyms:N--6-cyclohexyl-2(S)-isopropylhexanoyl>-L-isoleucyl>-2-pyridylmethylamine

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Chemical Property of N--6-cyclohexyl-2(S)-isopropylhexanoyl>-L-isoleucyl>-2-pyridylmethylamine

Chemical Property:

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Technology Process of N--6-cyclohexyl-2(S)-isopropylhexanoyl>-L-isoleucyl>-2-pyridylmethylamine

There total 3 articles about N--6-cyclohexyl-2(S)-isopropylhexanoyl>-L-isoleucyl>-2-pyridylmethylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 124322-00-5
N--5(S)-<(tert-butyloxycarbonyl)amino>-6-cyclohexyl-2(S)-isopropylhexanoyl>-L-isoleucyl>-2-pyridylmethylamine

: 132235-90-6
N--6-cyclohexyl-2(S)-isopropylhexanoyl>-L-isoleucyl>-2-pyridylmethylamine

Guidance literature:: With trifluoroacetic acid; In dichloromethane; for 0.75h;
DOI:10.1021/jm00108a006

Reference yield:

: 97920-16-6
N-L-isoleucyl-2-pyridylmethylamine

: 132235-90-6
N--6-cyclohexyl-2(S)-isopropylhexanoyl>-L-isoleucyl>-2-pyridylmethylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / diisopropylethylamine, diethylphosphoryl cyanide / CH₂Cl₂ / 16 h / 0 - 20 °C

2: 55 mg / trifluoroacetic acid / CH₂Cl₂ / 0.75 h

With diethylphosphoryl cyanide; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In dichloromethane;
DOI:10.1021/jm00108a006

Reference yield:

: 123471-30-7
4(S)-<(tert-butyldimethylsilyl)oxy>-5(S)-<(tert-butyloxycarbonyl)amino>-6-cyclohexyl-2(S)-isopropylhexanoic acid

: 132235-90-6
N--6-cyclohexyl-2(S)-isopropylhexanoyl>-L-isoleucyl>-2-pyridylmethylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / diisopropylethylamine, diethylphosphoryl cyanide / CH₂Cl₂ / 16 h / 0 - 20 °C

2: 55 mg / trifluoroacetic acid / CH₂Cl₂ / 0.75 h

With diethylphosphoryl cyanide; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In dichloromethane;
DOI:10.1021/jm00108a006