cycloheptanecarboxylic acid [4-(5-nitro-1H-benzoimidazol-2-yl)-phenyl]-amide

Base Information

• Chemical Name: cycloheptanecarboxylic acid [4-(5-nitro-1H-benzoimidazol-2-yl)-phenyl]-amide
• CAS No.: 1026982-71-7
• Molecular Formula: C₂₁H₂₂N₄O₃
• Molecular Weight: 378.431

Synonyms:cycloheptanecarboxylic acid [4-(5-nitro-1H-benzoimidazol-2-yl)-phenyl]-amide

Chemical Property of cycloheptanecarboxylic acid [4-(5-nitro-1H-benzoimidazol-2-yl)-phenyl]-amide

Chemical Property:

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Technology Process of cycloheptanecarboxylic acid [4-(5-nitro-1H-benzoimidazol-2-yl)-phenyl]-amide

There total 3 articles about cycloheptanecarboxylic acid [4-(5-nitro-1H-benzoimidazol-2-yl)-phenyl]-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-amino-benzoic acid (150-13-0,159246-81-8,8014-65-1) → cycloheptanecarboxylic acid [4-(5-nitro-1H-benzoimidazol-2-yl)-phenyl]-amide (1026982-71-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 47 percent / polyphosphoric acid / xylene / 60 - 150 °C

2: pyridine / 3 h / 20 °C

With pyridine; PPA; In xylene;

DOI:10.1016/j.ejmech.2006.03.014

Reference yield:

4-Nitrophenylene-1,2-diamine (99-56-9) → cycloheptanecarboxylic acid [4-(5-nitro-1H-benzoimidazol-2-yl)-phenyl]-amide (1026982-71-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 47 percent / polyphosphoric acid / xylene / 60 - 150 °C

2: pyridine / 3 h / 20 °C

With pyridine; PPA; In xylene;

DOI:10.1016/j.ejmech.2006.03.014

Reference yield:

cycloheptanecarbonyl chloride (6557-86-4) + 5(6)-nitro 2-(4-aminophenyl)-1H-benzimidazole (71002-88-5) → cycloheptanecarboxylic acid [4-(5-nitro-1H-benzoimidazol-2-yl)-phenyl]-amide (1026982-71-7)

Guidance literature:

With pyridine; at 20 ℃; for 3h;

DOI:10.1016/j.ejmech.2006.03.014

upstream raw materials:

cycloheptanecarbonyl chloride

5⁽⁶⁾-nitro 2-(4-aminophenyl)-1H-benzimidazole

4-amino-benzoic acid

4-Nitrophenylene-1,2-diamine

Downstream raw materials:

cycloheptanecarboxylic acid [4-(5-amino-1H-benzoimidazol-2-yl)-phenyl]-amide

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