p-octylbenzhydryl chloride

Base Information

• Chemical Name: p-octylbenzhydryl chloride
• CAS No.: 75812-80-5
• Molecular Formula: C₂₁H₂₇Cl
• Molecular Weight: 314.898
• Mol file: 75812-80-5.mol

Synonyms:p-octylbenzhydryl chloride

Chemical Property of p-octylbenzhydryl chloride

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of p-octylbenzhydryl chloride

There total 4 articles about p-octylbenzhydryl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

p-octylbenzhydrol (75812-79-2) → p-octylbenzhydryl chloride (75812-80-5)

Guidance literature:

With hydrogenchloride; magnesium sulfate; In benzene; Ambient temperature;

DOI:10.1021/jo00315a036

Reference yield:

Octylbenzene (2189-60-8) → p-octylbenzhydryl chloride (75812-80-5)

Guidance literature:

Multi-step reaction with 3 steps

1: 89 percent / AlCl₃ / CS₂ / 12 h / Heating

2: 87 percent / Zn, NaOH / aq. ethanol / 3 h / Heating

3: 98 percent / HCl, MgSO₄ / benzene / Ambient temperature

With hydrogenchloride; sodium hydroxide; aluminium trichloride; magnesium sulfate; zinc; In carbon disulfide; ethanol; benzene;

DOI:10.1021/jo00315a036

Reference yield:

n-octyl-4-benzophene (64357-43-3) → p-octylbenzhydryl chloride (75812-80-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 87 percent / Zn, NaOH / aq. ethanol / 3 h / Heating

2: 98 percent / HCl, MgSO₄ / benzene / Ambient temperature

With hydrogenchloride; sodium hydroxide; magnesium sulfate; zinc; In ethanol; benzene;

DOI:10.1021/jo00315a036

upstream raw materials:

p-octylbenzhydrol

Octylbenzene

n-octyl-4-benzophene

benzoyl chloride

Refernces