2-Hydroxy-2-tripyl-1-acenaphthenone

Base Information

• Chemical Name: 2-Hydroxy-2-tripyl-1-acenaphthenone
• CAS No.: 59261-61-9
• Molecular Formula: C₂₇H₃₀O₂
• Molecular Weight: 386.534
• Mol file: 59261-61-9.mol

Synonyms:2-Hydroxy-2-tripyl-1-acenaphthenone

Chemical Property of 2-Hydroxy-2-tripyl-1-acenaphthenone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of 2-Hydroxy-2-tripyl-1-acenaphthenone

There total 1 articles about 2-Hydroxy-2-tripyl-1-acenaphthenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(2,4,6-triisopropylphenyl)magnesium bromide (108894-99-1) + acenaphthene quinone (82-86-0) → 2-Hydroxy-2-tripyl-1-acenaphthenone (59261-61-9)

Guidance literature:

DOI:10.1021/ja00423a035

Reference yield:

2-Hydroxy-2-tripyl-1-acenaphthenone (59261-61-9) → 2-Tipyl-trans-1,2-acenaphthendiol

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; diethyl ether; ethyl acetate;

DOI:10.1021/ja00423a035

Reference yield:

2-Hydroxy-2-tripyl-1-acenaphthenone (59261-61-9) → trans-1-Phenyl-2-tipyl-1-acenaphthenol

Guidance literature:

Multi-step reaction with 3 steps

1: LiAlH₄ / diethyl ether; tetrahydrofuran; ethyl acetate

2: HCO₂H / acetic acid

3: benzene; pentane

With lithium aluminium tetrahydride; formic acid; In tetrahydrofuran; diethyl ether; acetic acid; ethyl acetate; pentane; benzene;

DOI:10.1021/ja00423a035

upstream raw materials:

(2,4,6-triisopropylphenyl)magnesium bromide

acenaphthene quinone

Downstream raw materials:

2-Tripyl-1-acenaphthenone