Technology Process of C50H74N2O17Si
There total 25 articles about C50H74N2O17Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
dmap; triethylamine;
In
dichloromethane;
at 20 ℃;
for 5h;
DOI:10.1002/anie.201203406
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: chromium dichloride / tetrahydrofuran / 2.33 h / 0 - 20 °C
2.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 4 h / -78 - 20 °C / Inert atmosphere
2.2: Inert atmosphere
3.1: water; methanesulfonamide; AD-mix-β / tert-butyl alcohol / 48 h / 0 °C
4.1: dmap; triethylamine / dichloromethane / 5 h / 20 °C
With
chromium dichloride; dmap; methanesulfonamide; AD-mix-β; water; triethylamine; 9-bora-bicyclo[3.3.1]nonane;
In
tetrahydrofuran; dichloromethane; tert-butyl alcohol;
1.1: |Takai-Utimoto Olefination / 2.2: |Suzuki-Miyaura Coupling;
DOI:10.1002/anie.201203406
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: ozone / dichloromethane / -78 °C
2.1: chromium dichloride / tetrahydrofuran / 2.33 h / 0 - 20 °C
3.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 4 h / -78 - 20 °C / Inert atmosphere
3.2: Inert atmosphere
4.1: water; methanesulfonamide; AD-mix-β / tert-butyl alcohol / 48 h / 0 °C
5.1: dmap; triethylamine / dichloromethane / 5 h / 20 °C
With
chromium dichloride; dmap; methanesulfonamide; AD-mix-β; water; ozone; triethylamine; 9-bora-bicyclo[3.3.1]nonane;
In
tetrahydrofuran; dichloromethane; tert-butyl alcohol;
2.1: |Takai-Utimoto Olefination / 3.2: |Suzuki-Miyaura Coupling;
DOI:10.1002/anie.201203406
