Phenyl 4-O-acetyl-6-O-benzyl-2-deoxy-3-O-(4-methoxybenzyl)-2-phthalimido-1-thio-β-D-glucopyranoside

Base Information

Chemical Name:Phenyl 4-O-acetyl-6-O-benzyl-2-deoxy-3-O-(4-methoxybenzyl)-2-phthalimido-1-thio-β-D-glucopyranoside
CAS No.:169962-29-2
Molecular Formula:C₃₇H₃₅NO₈S
Molecular Weight:653.753
Hs Code.:

Synonyms:Phenyl 4-O-acetyl-6-O-benzyl-2-deoxy-3-O-(4-methoxybenzyl)-2-phthalimido-1-thio-β-D-glucopyranoside

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Chemical Property of Phenyl 4-O-acetyl-6-O-benzyl-2-deoxy-3-O-(4-methoxybenzyl)-2-phthalimido-1-thio-β-D-glucopyranoside

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Technology Process of Phenyl 4-O-acetyl-6-O-benzyl-2-deoxy-3-O-(4-methoxybenzyl)-2-phthalimido-1-thio-β-D-glucopyranoside

There total 1 articles about Phenyl 4-O-acetyl-6-O-benzyl-2-deoxy-3-O-(4-methoxybenzyl)-2-phthalimido-1-thio-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 108-24-7
acetic anhydride

: Phenyl 6-O-benzyl-2-deoxy-3-O-(4-methoxybenzyl)-2-phthalimido-1-thio-β-D-glucopyranoside

: 169962-29-2
Phenyl 4-O-acetyl-6-O-benzyl-2-deoxy-3-O-(4-methoxybenzyl)-2-phthalimido-1-thio-β-D-glucopyranoside

Guidance literature:: With pyridine; for 16h; Ambient temperature;

Reference yield: 85.0%

: 169962-29-2
Phenyl 4-O-acetyl-6-O-benzyl-2-deoxy-3-O-(4-methoxybenzyl)-2-phthalimido-1-thio-β-D-glucopyranoside

: 288271-02-3
2-(trimethylsilyl)ethyl (2-acetamido-2-deoxy-3,4-O-isopropylidene-α-D-galactopyranosyl)-(1->3)-(2,4,6-tri-O-benzyl-β-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

: C₁₀₁H₁₁₆N₂O₂₄Si

Guidance literature:: Phenyl 4-O-acetyl-6-O-benzyl-2-deoxy-3-O-(4-methoxybenzyl)-2-phthalimido-1-thio-β-D-glucopyranoside; 2-(trimethylsilyl)ethyl (2-acetamido-2-deoxy-3,4-O-isopropylidene-α-D-galactopyranosyl)-(1->3)-(2,4,6-tri-O-benzyl-β-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside; In dichloromethane; at 20 ℃; for 3h;

With N-iodo-succinimide; trifluorormethanesulfonic acid; In dichloromethane; at -10 ℃; for 12h;
DOI:10.1016/j.tetasy.2005.02.013

Reference yield: 84.0%

: 158847-14-4
2-tetradecylhexadecan-1-ol

: 169962-29-2
Phenyl 4-O-acetyl-6-O-benzyl-2-deoxy-3-O-(4-methoxybenzyl)-2-phthalimido-1-thio-β-D-glucopyranoside

: 470462-14-7
2-(tetradecyl)hexadecyl 4-O-acetyl-6-O-benzyl-2-deoxy-3-O-(4-methoxybenzyl)-2-phthalimido-β-D-glucopyranoside

Guidance literature:: With N-iodo-succinimide; trifluorormethanesulfonic acid; 4 A molecular sieve; In dichloromethane; at 20 ℃; for 3h;
DOI:10.1081/CAR-120004336