(S)-2-((S)-3,3,3-Trifluoro-2-methoxy-2-phenyl-propionyloxy)-tridecanoic acid methyl ester

Base Information

Chemical Name:(S)-2-((S)-3,3,3-Trifluoro-2-methoxy-2-phenyl-propionyloxy)-tridecanoic acid methyl ester
CAS No.:96883-14-6
Molecular Formula:C₂₄H₃₅F₃O₅
Molecular Weight:460.534
Hs Code.:

Synonyms:(S)-2-((S)-3,3,3-Trifluoro-2-methoxy-2-phenyl-propionyloxy)-tridecanoic acid methyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-2-((S)-3,3,3-Trifluoro-2-methoxy-2-phenyl-propionyloxy)-tridecanoic acid methyl ester

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Technology Process of (S)-2-((S)-3,3,3-Trifluoro-2-methoxy-2-phenyl-propionyloxy)-tridecanoic acid methyl ester

There total 11 articles about (S)-2-((S)-3,3,3-Trifluoro-2-methoxy-2-phenyl-propionyloxy)-tridecanoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 20445-33-4,39637-99-5
(R)-methoxytrifluoromethylphenylacetyl chloride

: 96883-09-9
methyl (2S)-2-hydroxytridecanoate

: 96883-14-6
(S)-2-((S)-3,3,3-Trifluoro-2-methoxy-2-phenyl-propionyloxy)-tridecanoic acid methyl ester

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 20 ℃; for 18h; Inert atmosphere;
DOI:10.1021/ol901214n

Reference yield:

: 693-67-4
bromoundecane

: 96883-14-6
(S)-2-((S)-3,3,3-Trifluoro-2-methoxy-2-phenyl-propionyloxy)-tridecanoic acid methyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) NaOEt / 1.) EtOH, 30 min; RT 2.) reflux, 28 h

2: cc HCl / H₂O / Heating

3: 2N H₂SO₄, NaNO₂ / H₂O / 3 h / 90 - 93 °C

4: conc. HCl / benzene / 3 h / Heating

5: o.p.: 91.3percent

With hydrogenchloride; sulfuric acid; sodium ethanolate; sodium nitrite; In water; benzene;
DOI:10.1016/S0040-4020(01)96498-1

Reference yield:

: 35237-38-8
(+/-)-2-aminotridecenoic acid

: 96883-14-6
(S)-2-((S)-3,3,3-Trifluoro-2-methoxy-2-phenyl-propionyloxy)-tridecanoic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 2N H₂SO₄, NaNO₂ / H₂O / 3 h / 90 - 93 °C

2: conc. HCl / benzene / 3 h / Heating

3: o.p.: 91.3percent

With hydrogenchloride; sulfuric acid; sodium nitrite; In water; benzene;
DOI:10.1016/S0040-4020(01)96498-1