1-hydroxy-3-methyl-5-phenyl-2-pentene(β-acetoxy)ethyl sulfinate

Base Information

• Chemical Name: 1-hydroxy-3-methyl-5-phenyl-2-pentene(β-acetoxy)ethyl sulfinate
• CAS No.: 141244-65-7
• Molecular Formula: C₁₆H₂₂O₄S
• Molecular Weight: 310.414
• Mol file: 141244-65-7.mol

Synonyms:1-hydroxy-3-methyl-5-phenyl-2-pentene(β-acetoxy)ethyl sulfinate

Chemical Property of 1-hydroxy-3-methyl-5-phenyl-2-pentene(β-acetoxy)ethyl sulfinate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-hydroxy-3-methyl-5-phenyl-2-pentene(β-acetoxy)ethyl sulfinate

There total 3 articles about 1-hydroxy-3-methyl-5-phenyl-2-pentene(β-acetoxy)ethyl sulfinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

(E)-3-methyl-5-phenyl-pent-2-en-1-ol (72681-08-4) + 2-acetoxy-ethanesulfinyl chloride (106730-50-1) → 1-hydroxy-3-methyl-5-phenyl-2-pentene(β-acetoxy)ethyl sulfinate (141244-65-7)

Guidance literature:

With pyridine; In dichloromethane; at 20 ℃; for 1h;

Reference yield:

4-Phenyl-2-butanone (2550-26-7) → 1-hydroxy-3-methyl-5-phenyl-2-pentene(β-acetoxy)ethyl sulfinate (141244-65-7)

Guidance literature:

Multi-step reaction with 3 steps

1: NaH

2: LiAlH₄

3: 76 percent / pyridine / CH₂Cl₂ / 1 h / 20 °C

With pyridine; lithium aluminium tetrahydride; sodium hydride; In dichloromethane;

Reference yield:

ethyl (E)-3-methyl-5-phenylpent-2-enoate (36805-43-3) → 1-hydroxy-3-methyl-5-phenyl-2-pentene(β-acetoxy)ethyl sulfinate (141244-65-7)

Guidance literature:

Multi-step reaction with 2 steps

1: LiAlH₄

2: 76 percent / pyridine / CH₂Cl₂ / 1 h / 20 °C

With pyridine; lithium aluminium tetrahydride; In dichloromethane;

upstream raw materials:

(E)-3-methyl-5-phenyl-pent-2-en-1-ol

2-acetoxy-ethanesulfinyl chloride

4-Phenyl-2-butanone

ethyl (E)-3-methyl-5-phenylpent-2-enoate

Downstream raw materials:

3-methyl-5-phenyl-1-pentene-3(β-guanidino)ethyl sulfone-sulfonate

3-methyl-5-phenyl-1-pentene-3(β-amino)ethyl sulfone

3-methyl-5-phenyl-1-pentene-3(β-acetoxy)ethyl sulfone