ethyl (methyl-2,3,4-tri-O-benzyl-6,7-dideoxy-α-D-manno-octopyranosid)uranate

Base Information

Chemical Name:ethyl (methyl-2,3,4-tri-O-benzyl-6,7-dideoxy-α-D-manno-octopyranosid)uranate
CAS No.:232603-08-6
Molecular Formula:C₃₂H₃₈O₇
Molecular Weight:534.65
Hs Code.:

Synonyms:ethyl (methyl-2,3,4-tri-O-benzyl-6,7-dideoxy-α-D-manno-octopyranosid)uranate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl (methyl-2,3,4-tri-O-benzyl-6,7-dideoxy-α-D-manno-octopyranosid)uranate

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Technology Process of ethyl (methyl-2,3,4-tri-O-benzyl-6,7-dideoxy-α-D-manno-octopyranosid)uranate

There total 4 articles about ethyl (methyl-2,3,4-tri-O-benzyl-6,7-dideoxy-α-D-manno-octopyranosid)uranate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: (Z)-3-((2R,3R,4S,5S,6S)-3,4,5-Tris-benzyloxy-6-methoxy-tetrahydro-pyran-2-yl)-acrylic acid ethyl ester

: 232603-08-6
ethyl (methyl-2,3,4-tri-O-benzyl-6,7-dideoxy-α-D-manno-octopyranosid)uranate

Guidance literature:: With hydrogen; Lindlar's catalyst; In ethyl acetate; at 23 ℃; for 16h;
DOI:10.1021/ja961230+

Reference yield: 97.0%

: ethyl (methyl-6,7-dideoxy-α-D-manno-octo-6E-enopyranosid)uronate

: 232603-08-6
ethyl (methyl-2,3,4-tri-O-benzyl-6,7-dideoxy-α-D-manno-octopyranosid)uranate

Guidance literature:: With hydrogen; Lindlar's catalyst; In ethyl acetate; at 20 ℃; under 1810.07 Torr;
DOI:10.1021/jo0005159

Reference yield:

: 40653-15-4
methyl 2,3,4-tri-O-benzyl-α-D-manno-hexodialdo-1,5-pyranoside

: 232603-08-6
ethyl (methyl-2,3,4-tri-O-benzyl-6,7-dideoxy-α-D-manno-octopyranosid)uranate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.99 g / benzene / 20 °C

2: 97 percent / H₂ / Lindlar catalyst / ethyl acetate / 20 °C / 1810.07 Torr

With hydrogen; Lindlar's catalyst; In ethyl acetate; benzene; 1: Wittig reaction / 2: Catalytic hydrogenation;
DOI:10.1021/jo0005159