Dotriacontanedioic acid bis-[(R)-3-[(2-bromo-ethoxy)-(2-cyano-ethoxy)-phosphoryloxy]-2-(12-methoxy-dodecanoyloxy)-propyl] ester

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Chemical Name:Dotriacontanedioic acid bis-[(R)-3-[(2-bromo-ethoxy)-(2-cyano-ethoxy)-phosphoryloxy]-2-(12-methoxy-dodecanoyloxy)-propyl] ester
CAS No.:183145-30-4
Molecular Formula:C₇₄H₁₃₆Br₂N₂O₁₈P₂
Molecular Weight:1563.65
Hs Code.:

Synonyms:Dotriacontanedioic acid bis-[(R)-3-[(2-bromo-ethoxy)-(2-cyano-ethoxy)-phosphoryloxy]-2-(12-methoxy-dodecanoyloxy)-propyl] ester

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Chemical Property of Dotriacontanedioic acid bis-[(R)-3-[(2-bromo-ethoxy)-(2-cyano-ethoxy)-phosphoryloxy]-2-(12-methoxy-dodecanoyloxy)-propyl] ester

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Technology Process of Dotriacontanedioic acid bis-[(R)-3-[(2-bromo-ethoxy)-(2-cyano-ethoxy)-phosphoryloxy]-2-(12-methoxy-dodecanoyloxy)-propyl] ester

There total 1 articles about Dotriacontanedioic acid bis-[(R)-3-[(2-bromo-ethoxy)-(2-cyano-ethoxy)-phosphoryloxy]-2-(12-methoxy-dodecanoyloxy)-propyl] ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 92169-28-3
12-(methoxy)dodecanoic acid

: 183145-30-4
Dotriacontanedioic acid bis-[(R)-3-[(2-bromo-ethoxy)-(2-cyano-ethoxy)-phosphoryloxy]-2-(12-methoxy-dodecanoyloxy)-propyl] ester

Guidance literature:: Multi-step reaction with 4 steps

1: 72 percent / DMAP, 1,3-dicyclohexylcarbodiimide / CH₂Cl₂ / Ambient temperature

2: 95 percent / O₂, CuCl, TMEDA / xylene / 0.75 h / 140 - 150 °C

3: 95 percent / H₂ / Pd/C / ethanol; acetic acid / Ambient temperature

4: 1.) 1H-tetrazole, 2.) aq. H₂O₂ / 1) THF, rt, 30 min; 2) THF, 15 min

With 1H-tetrazole; dmap; N,N,N,N,-tetramethylethylenediamine; hydrogen; dihydrogen peroxide; oxygen; dicyclohexyl-carbodiimide; copper(l) chloride; palladium on activated charcoal; In ethanol; dichloromethane; acetic acid; xylene;
DOI:10.1021/jo9605455