[Cr(1,5,8,12-tetraaza-4-(1',1'-dimethylethyl)-2-(1'',1'',2'',2'',3'',3'',3''-heptafluoropropyl)-9,11-(dimethyl)-cyclotetradeca-1,4,8,11-tetraene)Cl₂]Cl

Base Information

• Chemical Name: [Cr(1,5,8,12-tetraaza-4-(1',1'-dimethylethyl)-2-(1'',1'',2'',2'',3'',3'',3''-heptafluoropropyl)-9,11-(dimethyl)-cyclotetradeca-1,4,8,11-tetraene)Cl₂]Cl
• CAS No.: 752205-27-9
• Molecular Formula: C₁₉H₂₇Cl₂CrF₇N₄*Cl
• Molecular Weight: 602.794
• Mol file: 752205-27-9.mol

Synonyms:[Cr(1,5,8,12-tetraaza-4-(1',1'-dimethylethyl)-2-(1'',1'',2'',2'',3'',3'',3''-heptafluoropropyl)-9,11-(dimethyl)-cyclotetradeca-1,4,8,11-tetraene)Cl₂]Cl

Chemical Property of [Cr(1,5,8,12-tetraaza-4-(1',1'-dimethylethyl)-2-(1'',1'',2'',2'',3'',3'',3''-heptafluoropropyl)-9,11-(dimethyl)-cyclotetradeca-1,4,8,11-tetraene)Cl₂]Cl

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of [Cr(1,5,8,12-tetraaza-4-(1',1'-dimethylethyl)-2-(1'',1'',2'',2'',3'',3'',3''-heptafluoropropyl)-9,11-(dimethyl)-cyclotetradeca-1,4,8,11-tetraene)Cl₂]Cl

There total 1 articles about [Cr(1,5,8,12-tetraaza-4-(1',1'-dimethylethyl)-2-(1'',1'',2'',2'',3'',3'',3''-heptafluoropropyl)-9,11-(dimethyl)-cyclotetradeca-1,4,8,11-tetraene)Cl₂]Cl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

1,5,8,12-tetraaza-4-(1',1'-dimethylethyl)-2-(1'',1'',2'',2'',3'',3'',3''-heptafluoropropyl)-9,11-(dimethyl)-cyclotetradeca-1,4,8,11-tetraene + chromium(III) chloride (10025-73-7,16284-59-6) → [Cr(1,5,8,12-tetraaza-4-(1',1'-dimethylethyl)-2-(1'',1'',2'',2'',3'',3'',3''-heptafluoropropyl)-9,11-(dimethyl)-cyclotetradeca-1,4,8,11-tetraene)Cl2]Cl (752205-27-9)

Guidance literature:

With HCl; In methanol; a ligand (10 mmol) was dissolved in a mixt. of methanol and HCl (concd.)and CrCl3 (10 mmol) in MeOH was added; the soln. was refluxed with stir ring for 12 h; the ppt. was filtered, washed with dry diethyl ether and dried in vac.; elem. anal.;

DOI:10.1081/SIM-120028305

upstream raw materials:

chromium(III) chloride