2-{1-[4-((E)-3,7-Dimethyl-octa-2,6-dienyloxy)-phenyl]-propoxy}-tetrahydro-pyran

Base Information

• Chemical Name: 2-{1-[4-((E)-3,7-Dimethyl-octa-2,6-dienyloxy)-phenyl]-propoxy}-tetrahydro-pyran
• CAS No.: 79727-54-1
• Molecular Formula: C₂₄H₃₆O₃
• Molecular Weight: 372.548

Synonyms:2-{1-[4-((E)-3,7-Dimethyl-octa-2,6-dienyloxy)-phenyl]-propoxy}-tetrahydro-pyran

Chemical Property of 2-{1-[4-((E)-3,7-Dimethyl-octa-2,6-dienyloxy)-phenyl]-propoxy}-tetrahydro-pyran

Chemical Property:

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Technology Process of 2-{1-[4-((E)-3,7-Dimethyl-octa-2,6-dienyloxy)-phenyl]-propoxy}-tetrahydro-pyran

There total 2 articles about 2-{1-[4-((E)-3,7-Dimethyl-octa-2,6-dienyloxy)-phenyl]-propoxy}-tetrahydro-pyran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

3,4-dihydro-2H-pyran (110-87-2) + 1-[4-((E)-3,7-Dimethyl-octa-2,6-dienyloxy)-phenyl]-propan-1-ol (79727-52-9) → 2-{1-[4-((E)-3,7-Dimethyl-octa-2,6-dienyloxy)-phenyl]-propoxy}-tetrahydro-pyran (79727-54-1)

Guidance literature:

toluene-4-sulfonic acid; for 0.166667h; Ambient temperature;

DOI:10.1135/cccc19811614

Reference yield:

4-(3,7-dimethyl-2,6-octadienyloxy)propiophenone (37087-78-8) → 2-{1-[4-((E)-3,7-Dimethyl-octa-2,6-dienyloxy)-phenyl]-propoxy}-tetrahydro-pyran (79727-54-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 80 percent / LiAlH₄ / diethyl ether / 0.5 h / Heating

2: 96 percent / p-toluenesulfonic acid / 0.17 h / Ambient temperature

With lithium aluminium tetrahydride; toluene-4-sulfonic acid; In diethyl ether;

DOI:10.1135/cccc19811614

Reference yield: 38.0%

2-{1-[4-((E)-3,7-Dimethyl-octa-2,6-dienyloxy)-phenyl]-propoxy}-tetrahydro-pyran (79727-54-1) → 2-(1-{4-[(E)-5-(3,3-Dimethyl-oxiranyl)-3-methyl-pent-2-enyloxy]-phenyl}-propoxy)-tetrahydro-pyran (79727-79-0)

Guidance literature:

With monoperoxyphthalic acid; In diethyl ether; at 10 - 20 ℃; for 0.5h;

DOI:10.1135/cccc19811614

upstream raw materials:

3,4-dihydro-2H-pyran

1-[4-((E)-3,7-Dimethyl-octa-2,6-dienyloxy)-phenyl]-propan-1-ol

4-(3,7-dimethyl-2,6-octadienyloxy)propiophenone

Downstream raw materials:

2-(1-{4-[(E)-5-(3,3-Dimethyl-oxiranyl)-3-methyl-pent-2-enyloxy]-phenyl}-propoxy)-tetrahydro-pyran

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