[(1,1'-ferrocenylene(NSitBuMe₂)2)La(tetrahydrofuran)(3,5-dimethylbenzyl)]

Base Information

Chemical Name:[(1,1'-ferrocenylene(NSitBuMe₂)2)La(tetrahydrofuran)(3,5-dimethylbenzyl)]
CAS No.:1204306-87-5
Molecular Formula:C₃₅H₅₇FeLaN₂OSi₂
Molecular Weight:772.774
Hs Code.:

[(1,1'-ferrocenylene(NSitBuMe<sub>2</sub>)2)La(tetrahydrofuran)(3,5-dimethylbenzyl)]

Synonyms:[(1,1'-ferrocenylene(NSitBuMe₂)2)La(tetrahydrofuran)(3,5-dimethylbenzyl)]

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Chemical Property of [(1,1'-ferrocenylene(NSitBuMe₂)2)La(tetrahydrofuran)(3,5-dimethylbenzyl)]

Chemical Property:

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Technology Process of [(1,1'-ferrocenylene(NSitBuMe₂)2)La(tetrahydrofuran)(3,5-dimethylbenzyl)]

There total 1 articles about [(1,1'-ferrocenylene(NSitBuMe₂)2)La(tetrahydrofuran)(3,5-dimethylbenzyl)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.3%

: 944466-36-8
1,1′-bis-(tert-butyldimethylsilylamino)ferrocene

: 1204306-86-4
La(tetrahydrofuran)3(CH₂C₆H₃Me₂-3,5)3

: 1204306-87-5
[(1,1'-ferrocenylene(NSitBuMe₂)2)La(tetrahydrofuran)(3,5-dimethylbenzyl)]

Guidance literature:: In tetrahydrofuran; diethyl ether; (N2); mixing soln. of lanthanum compd. in 1:1 THF/diethyl ether and ferrocene deriv. in ether at -35°C, stirring for 3 h at 0°C; evapn., washing with hexane, extn. (toluene/hexane (1:1)), filtration though celite, evapn., dissolving in diethyl ether, layering with pentane,keeping at -35°C, isolation of crystals by decantation, elem. an al.;
DOI:10.1021/ja908489p

Reference yield:

: 119-65-3
isoquinoline

: 1204306-87-5
[(1,1'-ferrocenylene(NSitBuMe₂)2)La(tetrahydrofuran)(3,5-dimethylbenzyl)]

: 1204306-73-9
[(1,1'-ferrocenylene(NSi(tBu)Me₂)2)La(tetrahydrofuran)2(C₉H₈N)]

: [(1,1'-ferrocenylene(NSitBuMe₂)2)La(tetrahydrofuran)(1-(3,5-dimethylbenzyl)isoquinoline(-H))]

Guidance literature:: In benzene-d6; byproducts: C6H3(CH3)3; (N2); mixing 1 equiv. of lanthanum compd. and 1 equiv. of isoquinoline in C6D6, heating at 50°C for 96 h; X-ray anal.;
DOI:10.1021/ja908489p