2-bromo-6-tert-butyldimethylsilyl-4-fluorophenyl trifluoromethanesulfonate

Base Information

Chemical Name:2-bromo-6-tert-butyldimethylsilyl-4-fluorophenyl trifluoromethanesulfonate
CAS No.:1089665-88-2
Molecular Formula:C₁₃H₁₇BrF₄O₃SSi
Molecular Weight:437.325
Hs Code.:

Synonyms:2-bromo-6-tert-butyldimethylsilyl-4-fluorophenyl trifluoromethanesulfonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-bromo-6-tert-butyldimethylsilyl-4-fluorophenyl trifluoromethanesulfonate

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Technology Process of 2-bromo-6-tert-butyldimethylsilyl-4-fluorophenyl trifluoromethanesulfonate

There total 1 articles about 2-bromo-6-tert-butyldimethylsilyl-4-fluorophenyl trifluoromethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 358-23-6
trifluoromethylsulfonic anhydride

: 1089665-87-1
2-bromo-6-tert-butyldimethylsilyl-4-fluorophenol

: 1089665-88-2
2-bromo-6-tert-butyldimethylsilyl-4-fluorophenyl trifluoromethanesulfonate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 - 20 ℃; for 9.5h; Inert atmosphere;
DOI:10.1002/anie.200803011

Reference yield: 49.0%

: 1578-33-2
2-furyltrimethylsilane

: 1089665-88-2
2-bromo-6-tert-butyldimethylsilyl-4-fluorophenyl trifluoromethanesulfonate

: 1089666-16-9
5-tert-butyldimethylsilyl-1,4-epoxy-7-fluoro-1-trimethylsilyl-1,4-dihydronaphthalene

Guidance literature:: With n-butyllithium; In hexane; toluene; at -78 ℃; for 0.333333h; optical yield given as %de; regioselective reaction; Inert atmosphere;
DOI:10.1002/anie.200803011