2,2'-di-O-benzoyl-4,6:4',6'-di-O-benzylidene-3,3'-dideoxy-α,α-D-trehalose

Base Information

Chemical Name:2,2'-di-O-benzoyl-4,6:4',6'-di-O-benzylidene-3,3'-dideoxy-α,α-D-trehalose
CAS No.:36026-59-2
Molecular Formula:C₄₀H₃₈O₁₁
Molecular Weight:694.735
Hs Code.:

Synonyms:2,2'-di-O-benzoyl-4,6:4',6'-di-O-benzylidene-3,3'-dideoxy-α,α-D-trehalose

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Chemical Property of 2,2'-di-O-benzoyl-4,6:4',6'-di-O-benzylidene-3,3'-dideoxy-α,α-D-trehalose

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Technology Process of 2,2'-di-O-benzoyl-4,6:4',6'-di-O-benzylidene-3,3'-dideoxy-α,α-D-trehalose

There total 4 articles about 2,2'-di-O-benzoyl-4,6:4',6'-di-O-benzylidene-3,3'-dideoxy-α,α-D-trehalose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: C₅₄H₄₆O₁₅S₂

: 36026-59-2
2,2'-di-O-benzoyl-4,6:4',6'-di-O-benzylidene-3,3'-dideoxy-α,α-D-trehalose

Guidance literature:: With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In toluene; for 0.5h; Heating;
DOI:10.1016/j.carres.2007.05.009

Reference yield:

: 613-90-1
benzoyl cyanide

: 36026-59-2
2,2'-di-O-benzoyl-4,6:4',6'-di-O-benzylidene-3,3'-dideoxy-α,α-D-trehalose

Guidance literature:: Multi-step reaction with 3 steps

1: 45 percent / Et₃N / acetonitrile / 2 h

2: 80 percent / DMAP / acetonitrile / 20 °C

3: 84 percent / AIBN; Bu₃SnH / toluene / 0.5 h / Heating

With dmap; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; triethylamine; In toluene; acetonitrile;
DOI:10.1016/j.carres.2007.05.009

Reference yield:

: 18929-82-3
4,6-O-benzylidene-α-D-glucopyranosyl-(1→1)-4',6'-O-benzylidene-α-D-glucopyranoside

: 36026-59-2
2,2'-di-O-benzoyl-4,6:4',6'-di-O-benzylidene-3,3'-dideoxy-α,α-D-trehalose

Guidance literature:: Multi-step reaction with 3 steps

1: 45 percent / Et₃N / acetonitrile / 2 h

2: 80 percent / DMAP / acetonitrile / 20 °C

3: 84 percent / AIBN; Bu₃SnH / toluene / 0.5 h / Heating

With dmap; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; triethylamine; In toluene; acetonitrile;
DOI:10.1016/j.carres.2007.05.009