C₃₃H₃₇NO₉

Base Information

Chemical Name:C₃₃H₃₇NO₉
CAS No.:1493759-38-8
Molecular Formula:C₃₃H₃₇NO₉
Molecular Weight:591.658
Hs Code.:

C<sub>33</sub>H<sub>37</sub>NO<sub>9</sub>

Synonyms:C₃₃H₃₇NO₉

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Chemical Property of C₃₃H₃₇NO₉

Chemical Property:

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Technology Process of C₃₃H₃₇NO₉

There total 7 articles about C₃₃H₃₇NO₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 496-15-1
1-indoline

: 1493759-38-8
C₃₃H₃₇NO₉

Guidance literature:: Multi-step reaction with 6 steps

1.1: ethanol; water / Reflux; Inert atmosphere

2.1: pyridine; dmap / chloroform / 20 °C

3.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / water; 1,4-dioxane / 20 °C

4.1: trichlorophosphate / 1,2-dichloro-ethane / 70 °C

5.1: magnesium; ethylene dibromide / tetrahydrofuran / 20 °C / Inert atmosphere

5.2: Inert atmosphere; Cooling with ice

6.1: triethylsilane; boron trifluoride diethyl etherate / dichloromethane; acetonitrile / Inert atmosphere; Cooling with ice

With pyridine; triethylsilane; dmap; boron trifluoride diethyl etherate; magnesium; ethylene dibromide; 2,3-dicyano-5,6-dichloro-p-benzoquinone; trichlorophosphate; In tetrahydrofuran; 1,4-dioxane; ethanol; dichloromethane; chloroform; water; 1,2-dichloro-ethane; acetonitrile; 4.1: |Vilsmeier-Haack Formylation;
DOI:10.1021/ml400339b

Reference yield:

: 22855-03-4,23477-48-7,38730-31-3,38740-49-7
1-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)indoline

: 1493759-38-8
C₃₃H₃₇NO₉

Guidance literature:: Multi-step reaction with 4 steps

1.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / water; 1,4-dioxane / 20 °C

2.1: trichlorophosphate / 1,2-dichloro-ethane / 70 °C

3.1: magnesium; ethylene dibromide / tetrahydrofuran / 20 °C / Inert atmosphere

3.2: Inert atmosphere; Cooling with ice

4.1: triethylsilane; boron trifluoride diethyl etherate / dichloromethane; acetonitrile / Inert atmosphere; Cooling with ice

With triethylsilane; boron trifluoride diethyl etherate; magnesium; ethylene dibromide; 2,3-dicyano-5,6-dichloro-p-benzoquinone; trichlorophosphate; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water; 1,2-dichloro-ethane; acetonitrile; 2.1: |Vilsmeier-Haack Formylation;
DOI:10.1021/ml400339b

Reference yield:

: 5059-38-1,23392-14-5,58918-52-8
1-(2',3',4',6'-tetra-O-acetyl-β-D-glucopyranosyl)-1H-indole

: 1493759-38-8
C₃₃H₃₇NO₉

Guidance literature:: Multi-step reaction with 3 steps

1.1: trichlorophosphate / 1,2-dichloro-ethane / 70 °C

2.1: magnesium; ethylene dibromide / tetrahydrofuran / 20 °C / Inert atmosphere

2.2: Inert atmosphere; Cooling with ice

3.1: triethylsilane; boron trifluoride diethyl etherate / dichloromethane; acetonitrile / Inert atmosphere; Cooling with ice

With triethylsilane; boron trifluoride diethyl etherate; magnesium; ethylene dibromide; trichlorophosphate; In tetrahydrofuran; dichloromethane; 1,2-dichloro-ethane; acetonitrile; 1.1: |Vilsmeier-Haack Formylation;
DOI:10.1021/ml400339b