benzyloxycarbonyl-L-phenylalanyl-L-prolyl-D-alanyl-L-phenylalanyl-L-prolyl-D-alanine methyl ester

Base Information

• Chemical Name: benzyloxycarbonyl-L-phenylalanyl-L-prolyl-D-alanyl-L-phenylalanyl-L-prolyl-D-alanine methyl ester
• CAS No.: 90107-61-2
• Molecular Formula: C₄₃H₅₂N₆O₉
• Molecular Weight: 796.921

Synonyms:benzyloxycarbonyl-L-phenylalanyl-L-prolyl-D-alanyl-L-phenylalanyl-L-prolyl-D-alanine methyl ester

Chemical Property of benzyloxycarbonyl-L-phenylalanyl-L-prolyl-D-alanyl-L-phenylalanyl-L-prolyl-D-alanine methyl ester

Chemical Property:

Purity/Quality:

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Technology Process of benzyloxycarbonyl-L-phenylalanyl-L-prolyl-D-alanyl-L-phenylalanyl-L-prolyl-D-alanine methyl ester

There total 4 articles about benzyloxycarbonyl-L-phenylalanyl-L-prolyl-D-alanyl-L-phenylalanyl-L-prolyl-D-alanine methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-(benzyloxycarbonyl)-phenylalanine-N-hydroxysuccinimide ester (3397-32-8) → benzyloxycarbonyl-L-phenylalanyl-L-prolyl-D-alanyl-L-phenylalanyl-L-prolyl-D-alanine methyl ester (90107-61-2)

Guidance literature:

Multi-step reaction with 3 steps

1: dimethylformamide

2: H₂ / Pd-C / methanol

3: 1.) DMF; 2.) DMF

With hydrogen; palladium on activated charcoal; In methanol; N,N-dimethyl-formamide;

DOI:10.1021/ja00325a023

Reference yield:

benzyloxycarbonyl-L-phenylalanyl-L-prolyl-D-alanine methyl ester (90107-58-7) → benzyloxycarbonyl-L-phenylalanyl-L-prolyl-D-alanyl-L-phenylalanyl-L-prolyl-D-alanine methyl ester (90107-61-2)

Guidance literature:

Multi-step reaction with 2 steps

1: H₂ / Pd-C / methanol

2: 1.) DMF; 2.) DMF

With hydrogen; palladium on activated charcoal; In methanol;

DOI:10.1021/ja00325a023

Reference yield:

Pro-D-Ala-OMe hydrochloride (90107-57-6) → benzyloxycarbonyl-L-phenylalanyl-L-prolyl-D-alanyl-L-phenylalanyl-L-prolyl-D-alanine methyl ester (90107-61-2)

Guidance literature:

Multi-step reaction with 3 steps

1: dimethylformamide

2: H₂ / Pd-C / methanol

3: 1.) DMF; 2.) DMF

With hydrogen; palladium on activated charcoal; In methanol; N,N-dimethyl-formamide;

DOI:10.1021/ja00325a023

upstream raw materials:

L-phenylalanyl-L-prolyl-D-alanine methyl ester

benzyloxycarbonyl-L-phenylalanyl-L-prolyl-D-alanine hydrazide

N-(benzyloxycarbonyl)-phenylalanine-N-hydroxysuccinimide ester

Pro-D-Ala-OMe hydrochloride

Downstream raw materials:

cyclo(L-Phe-L-Pro-D-Ala)2

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