(E)-1-(4-chlorophenyl)-2-(4-(4-methoxyphenyl)butan-2-ylidene)hydrazine

Base Information

Chemical Name:(E)-1-(4-chlorophenyl)-2-(4-(4-methoxyphenyl)butan-2-ylidene)hydrazine
CAS No.:1381772-13-9
Molecular Formula:C₁₇H₁₉ClN₂O
Molecular Weight:302.804
Hs Code.:

Synonyms:(E)-1-(4-chlorophenyl)-2-(4-(4-methoxyphenyl)butan-2-ylidene)hydrazine

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Chemical Property of (E)-1-(4-chlorophenyl)-2-(4-(4-methoxyphenyl)butan-2-ylidene)hydrazine

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Technology Process of (E)-1-(4-chlorophenyl)-2-(4-(4-methoxyphenyl)butan-2-ylidene)hydrazine

There total 1 articles about (E)-1-(4-chlorophenyl)-2-(4-(4-methoxyphenyl)butan-2-ylidene)hydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 104-20-1
4-(4-methoxyphenyl)-2-butanone

: 1073-69-4
N-4-chlorophenylhydrazine

: 1381772-16-2
(Z)-1-(4-chlorophenyl)-2-(4-(4-methoxyphenyl)butan-2-ylidene)hydrazine

: 1381772-13-9
(E)-1-(4-chlorophenyl)-2-(4-(4-methoxyphenyl)butan-2-ylidene)hydrazine

Guidance literature:: In dichloromethane; for 17h; Molecular sieve; Inert atmosphere; Reflux;
DOI:10.1021/ja303054c

Reference yield: 93.0%

: 1381772-13-9
(E)-1-(4-chlorophenyl)-2-(4-(4-methoxyphenyl)butan-2-ylidene)hydrazine

: 1381772-50-4
(E)-1-(2-chloro-4-(4-methoxyphenyl)butan-2-yl)-2-(4-chlorophenyl)diazene

Guidance literature:: (E)-1-(4-chlorophenyl)-2-(4-(4-methoxyphenyl)butan-2-ylidene)hydrazine; With oxalyl dichloride; dimethyl sulfoxide; In tetrahydrofuran; at -78 - -55 ℃; for 0.166667h; Inert atmosphere;

With triethylamine; In tetrahydrofuran; at 25 ℃; for 0.0833333h; Inert atmosphere;
DOI:10.1021/ja303054c

Reference yield:

: 1381772-13-9
(E)-1-(4-chlorophenyl)-2-(4-(4-methoxyphenyl)butan-2-ylidene)hydrazine

: 1381772-74-2
1-(4-chlorophenyl)-5-(4-methoxyphenyl)-3-methyl-4,5-dihydro-1H-pyrazole

Guidance literature:: Multi-step reaction with 2 steps

1.1: oxalyl dichloride; dimethyl sulfoxide / tetrahydrofuran / 0.17 h / -78 - -55 °C / Inert atmosphere

1.2: 0.08 h / 25 °C / Inert atmosphere

2.1: aluminum (III) chloride / dichloromethane / 4 h / -60 °C / Inert atmosphere

2.2: 0 - 20 °C / Inert atmosphere

With aluminum (III) chloride; oxalyl dichloride; dimethyl sulfoxide; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ja303054c