benzyl cyclopentylcarbamate

Base Information

• Chemical Name: benzyl cyclopentylcarbamate
• CAS No.: 909906-70-3
• Molecular Formula: C₁₃H₁₇NO₂
• Molecular Weight: 219.283
• Mol file: 909906-70-3.mol

Synonyms:benzyl cyclopentylcarbamate

Chemical Property of benzyl cyclopentylcarbamate

Chemical Property:

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Technology Process of benzyl cyclopentylcarbamate

There total 5 articles about benzyl cyclopentylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

N-(Benzyloxycarbonyloxy)succinimide (13139-17-8) + Cyclopentamine (1003-03-8) → benzyl cyclopentylcarbamate (909906-70-3)

Guidance literature:

With 1-butyl-3-methylimidazolium Tetrafluoroborate; In neat (no solvent); at 25 ℃; for 0.05h;

DOI:10.1039/c5ra12121c

Reference yield: 72.0%

5-propyl-benzo[1,3]dioxol-2-one + Cyclopentamine (1003-03-8) + benzyl alcohol (100-51-6,185532-71-2) → benzyl cyclopentylcarbamate (909906-70-3)

Guidance literature:

5-propyl-benzo[1,3]dioxol-2-one; benzyl alcohol; With zinc(II) acetate dihydrate; at 50 ℃; for 16h; Sealed tube;

Cyclopentamine; In 2-methyltetrahydrofuran; at 25 ℃; for 16h; Sealed tube;

DOI:10.1002/cssc.201900406

Reference yield: 67.0%

O-benzyl carbamate (621-84-1) + cyclopentanone (120-92-3) → benzyl cyclopentylcarbamate (909906-70-3) + Cyclopentanol (96-41-3)

Guidance literature:

With triethylsilane; sodium hexaflorophosphate; perrhenic acid anhydride; In dichloromethane; at 50 ℃; for 24h; chemoselective reaction;

DOI:10.1039/c3ob40918j

upstream raw materials:

O-benzyl carbamate

cyclopentanone

N-(Benzyloxycarbonyloxy)succinimide

Cyclopentamine