3-<<4-phenyl>thio>propanoic acid

Base Information

Chemical Name:3-<<4-phenyl>thio>propanoic acid
CAS No.:130198-96-8
Molecular Formula:C₁₃H₁₇Cl₂NO₂S
Molecular Weight:322.255
Hs Code.:

3-<<4-<N,N-bis(2-chloroethyl)amino>phenyl>thio>propanoic acid

Synonyms:3-<<4-phenyl>thio>propanoic acid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-<<4-phenyl>thio>propanoic acid

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Technology Process of 3-<<4-phenyl>thio>propanoic acid

There total 8 articles about 3-<<4-phenyl>thio>propanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 130198-90-2
methyl 3-<<4-phenyl>thio>propionate

: 130198-96-8
3-<<4-phenyl>thio>propanoic acid

Guidance literature:: With hydrogenchloride; for 1.5h; Heating;
DOI:10.1021/jm00173a016

Reference yield:

: 100132-31-8
4-benzenethiol

: 130198-96-8
3-<<4-phenyl>thio>propanoic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 57 percent / K₂CO₃ / methanol / 0.17 h / Heating

2: Et₃N / CH₂Cl₂ / 0.75 h / 0 °C

3: NaCl / dimethylformamide / 0.08 h / 120 °C

4: 73 percent / concd. HCl / 1.5 h / Heating

With hydrogenchloride; potassium carbonate; triethylamine; sodium chloride; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm00173a016

Reference yield:

: 130219-46-4
S-<(benzyloxy)carbonyl>-4-aminobenzenethiol

: 130198-96-8
3-<<4-phenyl>thio>propanoic acid

Guidance literature:: Multi-step reaction with 6 steps

1: 79 percent / AcOH / tetrahydrofuran / 336 h / 20 °C

2: 56 percent / NaOH / ethanol / 2 h / Heating

3: 57 percent / K₂CO₃ / methanol / 0.17 h / Heating

4: Et₃N / CH₂Cl₂ / 0.75 h / 0 °C

5: NaCl / dimethylformamide / 0.08 h / 120 °C

6: 73 percent / concd. HCl / 1.5 h / Heating

With hydrogenchloride; sodium hydroxide; potassium carbonate; acetic acid; triethylamine; sodium chloride; In tetrahydrofuran; methanol; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm00173a016