2-{4-[1-(tert-butoxycarbonyl)-3-pyrazoyl]phenyl}-6-(tributylstannyl)-imidazo[1,2-a]pyridine

Base Information

Chemical Name:2-{4-[1-(tert-butoxycarbonyl)-3-pyrazoyl]phenyl}-6-(tributylstannyl)-imidazo[1,2-a]pyridine
CAS No.:938461-50-8
Molecular Formula:C₃₃H₄₆N₄O₂Sn
Molecular Weight:649.464
Hs Code.:

Synonyms:2-{4-[1-(tert-butoxycarbonyl)-3-pyrazoyl]phenyl}-6-(tributylstannyl)-imidazo[1,2-a]pyridine

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Chemical Property of 2-{4-[1-(tert-butoxycarbonyl)-3-pyrazoyl]phenyl}-6-(tributylstannyl)-imidazo[1,2-a]pyridine

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Technology Process of 2-{4-[1-(tert-butoxycarbonyl)-3-pyrazoyl]phenyl}-6-(tributylstannyl)-imidazo[1,2-a]pyridine

There total 1 articles about 2-{4-[1-(tert-butoxycarbonyl)-3-pyrazoyl]phenyl}-6-(tributylstannyl)-imidazo[1,2-a]pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 938461-48-4
2-[4-(1H-3-pyrazolyl)phenyl]-6-(tributylstannyl)imidazo[1,2-a]pyridine

: 24424-99-5
di-tert-butyl dicarbonate

: 938461-50-8
2-{4-[1-(tert-butoxycarbonyl)-3-pyrazoyl]phenyl}-6-(tributylstannyl)-imidazo[1,2-a]pyridine

Guidance literature:: In dichloromethane; at 0 - 20 ℃; for 8h;
DOI:10.1016/j.bmc.2014.05.043

Reference yield:

: 938461-50-8
2-{4-[1-(tert-butoxycarbonyl)-3-pyrazoyl]phenyl}-6-(tributylstannyl)-imidazo[1,2-a]pyridine

: 938461-49-5
[123I] 6-iodo-2-[4-(1H-3-pyrazolyl)phenyl]imidazo[1,2-a]pyridine

Guidance literature:: With [¹²³I] sodium iodide; chloroamine-T; sodium iodide; In water; isopropyl alcohol; at 20 ℃; for 0.0833333h; pH=5.5; Sodium phosphate buffer;

Reference yield:

: 938461-50-8
2-{4-[1-(tert-butoxycarbonyl)-3-pyrazoyl]phenyl}-6-(tributylstannyl)-imidazo[1,2-a]pyridine

: 938460-58-3
6-iodo-2-[4-(1H-3-pyrazolyl)phenyl]imidazo[1,2-a]pyridine

Guidance literature:: 2-{4-[1-(tert-butoxycarbonyl)-3-pyrazoyl]phenyl}-6-(tributylstannyl)-imidazo[1,2-a]pyridine; With chloroamine-T; sodium iodide; In aq. phosphate buffer; at 20 ℃;

With sodium hydroxide; In aq. phosphate buffer; ethanol; for 0.583333h; Heating;
DOI:10.1016/j.bmc.2014.05.043