3-O-benzyl-1,2-isopropylidene-6-O-triphenylmethyl-α-D-allo-hexofuran-5-ulose

Base Information

Chemical Name:3-O-benzyl-1,2-isopropylidene-6-O-triphenylmethyl-α-D-allo-hexofuran-5-ulose
CAS No.:106734-68-3
Molecular Formula:C₃₅H₃₆O₆
Molecular Weight:552.667
Hs Code.:

Synonyms:3-O-benzyl-1,2-isopropylidene-6-O-triphenylmethyl-α-D-allo-hexofuran-5-ulose

Suppliers and Price of 3-O-benzyl-1,2-isopropylidene-6-O-triphenylmethyl-α-D-allo-hexofuran-5-ulose

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-O-benzyl-1,2-isopropylidene-6-O-triphenylmethyl-α-D-allo-hexofuran-5-ulose

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Technology Process of 3-O-benzyl-1,2-isopropylidene-6-O-triphenylmethyl-α-D-allo-hexofuran-5-ulose

There total 8 articles about 3-O-benzyl-1,2-isopropylidene-6-O-triphenylmethyl-α-D-allo-hexofuran-5-ulose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 57099-04-4
3-O-benzyl-1,2-O-isopropylidene-α-D-allofuranose

: 76-83-5
trityl chloride

: 106734-68-3
3-O-benzyl-1,2-isopropylidene-6-O-triphenylmethyl-α-D-allo-hexofuran-5-ulose

Guidance literature:: With triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 14h;
DOI:10.1007/s00706-009-0171-1

Reference yield: 65.0%

: 76-83-5
trityl chloride

: 42926-89-6
1,2-O-isopropylidene-3-O-benzyl-α-D-glucofuranose

: 35777-80-1,37073-70-4,106734-68-3,106734-69-4
3-O-Benzyl-1,2-O-isopropyliden-6-O-triphenylmethyl-α-D-glucofuranose

Guidance literature:: With pyridine; for 12h; Inert atmosphere;
DOI:10.1039/c3ra43827a

Reference yield:

: 14686-89-6
(1,2:5,6)-di-O-isopropylidene-D-gulose

: 106734-68-3
3-O-benzyl-1,2-isopropylidene-6-O-triphenylmethyl-α-D-allo-hexofuran-5-ulose

Guidance literature:: Multi-step reaction with 3 steps

1: NaH, Bu₄NI / tetrahydrofuran / 2 h / Ambient temperature

2: 0.06 N HCl / methanol / 2 h / 55 °C

3: pyridine / dimethylformamide / 12 h / Ambient temperature

With pyridine; hydrogenchloride; tetra-(n-butyl)ammonium iodide; sodium hydride; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(00)79338-5