(1RS)-2-benzoyl-1,2,3,4-tetrahydro-1-(3,3,3-trichloro-2-oxopropyl)-β-carboline

Base Information

Chemical Name:(1RS)-2-benzoyl-1,2,3,4-tetrahydro-1-(3,3,3-trichloro-2-oxopropyl)-β-carboline
CAS No.:142656-12-0
Molecular Formula:C₂₁H₁₇Cl₃N₂O₂
Molecular Weight:435.737
Hs Code.:

Synonyms:(1RS)-2-benzoyl-1,2,3,4-tetrahydro-1-(3,3,3-trichloro-2-oxopropyl)-β-carboline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1RS)-2-benzoyl-1,2,3,4-tetrahydro-1-(3,3,3-trichloro-2-oxopropyl)-β-carboline

Chemical Property:

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Technology Process of (1RS)-2-benzoyl-1,2,3,4-tetrahydro-1-(3,3,3-trichloro-2-oxopropyl)-β-carboline

There total 3 articles about (1RS)-2-benzoyl-1,2,3,4-tetrahydro-1-(3,3,3-trichloro-2-oxopropyl)-β-carboline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 142656-06-2
4-amino>-1,1,1-trichloro-3-buten-2-one

: 142656-12-0
(1RS)-2-benzoyl-1,2,3,4-tetrahydro-1-(3,3,3-trichloro-2-oxopropyl)-β-carboline

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 0 ℃; for 0.333333h;

Reference yield:

: 61-54-1
tryptamine

: 142656-12-0
(1RS)-2-benzoyl-1,2,3,4-tetrahydro-1-(3,3,3-trichloro-2-oxopropyl)-β-carboline

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / tetrahydrofuran / 24 h / Ambient temperature

2: 81 percent / pyridine / CH₂Cl₂ / 12 h / Ambient temperature

3: 86 percent / trifluoroacetic acid / CH₂Cl₂ / 0.33 h / 0 °C

With pyridine; trifluoroacetic acid; In tetrahydrofuran; dichloromethane;

Reference yield:

: 142656-04-0
1,1,1-trichloro-4-<2-(3-inolyl)ethylamino>-3-buten-2-one

: 142656-12-0
(1RS)-2-benzoyl-1,2,3,4-tetrahydro-1-(3,3,3-trichloro-2-oxopropyl)-β-carboline

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / pyridine / CH₂Cl₂ / 12 h / Ambient temperature

2: 86 percent / trifluoroacetic acid / CH₂Cl₂ / 0.33 h / 0 °C

With pyridine; trifluoroacetic acid; In dichloromethane;