N,N-diethyl-O-mesitylenesulfonylhydroxylamine

Base Information

• Chemical Name: N,N-diethyl-O-mesitylenesulfonylhydroxylamine
• CAS No.: 67530-31-8
• Molecular Formula: C₁₃H₂₁NO₃S
• Molecular Weight: 271.381
• Mol file: 67530-31-8.mol

Synonyms:N,N-diethyl-O-mesitylenesulfonylhydroxylamine

Chemical Property of N,N-diethyl-O-mesitylenesulfonylhydroxylamine

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of N,N-diethyl-O-mesitylenesulfonylhydroxylamine

There total 1 articles about N,N-diethyl-O-mesitylenesulfonylhydroxylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

2-mesitylenesulphonyl chloride (773-64-8) + triethylamine (121-44-8) → N,N-diethyl-O-mesitylenesulfonylhydroxylamine (67530-31-8)

Guidance literature:

With N-ethyl-N-hydroxy-ethanamine; In dichloromethane; at -25 ℃; for 2.5h;

DOI:10.1016/0040-4020(82)85082-5

Reference yield:

N,N-diethyl-O-mesitylenesulfonylhydroxylamine (67530-31-8) + 1,2,3-Triphenylallyl-anion → N.N-Diethyltriphenylallylamin (67530-39-6)

Guidance literature:

In diethyl ether;

upstream raw materials:

2-mesitylenesulphonyl chloride

triethylamine

Downstream raw materials:

N_.N-Diethyltriphenylallylamin