N-tert-Butylglyoxylsaeureamid

Base Information

• Chemical Name: N-tert-Butylglyoxylsaeureamid
• CAS No.: 153716-05-3
• Molecular Formula: C₆H₁₁NO₂
• Molecular Weight: 129.159

Synonyms:N-tert-Butylglyoxylsaeureamid

Chemical Property of N-tert-Butylglyoxylsaeureamid

Chemical Property:

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Technology Process of N-tert-Butylglyoxylsaeureamid

There total 1 articles about N-tert-Butylglyoxylsaeureamid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-acetamido-N-tert-butylacetamide → 2-acetamido-N-tert-butyl-2-hydroxyacetamide (957825-89-7) + N1-acetyl-N2-tert-butyloxalamide (957825-90-0) + N-Acetyl formamide (21163-79-1) + N-tert-Butylglyoxylsaeureamid (153716-05-3)

Guidance literature:

With Oxone; In water; acetonitrile; at 25 ℃; Kinetics;

DOI:10.1021/ja075075i

Reference yield: 69.0%

piperidine (110-89-4) + N-tert-Butylglyoxylsaeureamid (153716-05-3) → piperidine hydrochloride (6091-44-7) + 1-(tert-butylcarbamoyl-methylene)-piperidinium; chloride

Guidance literature:

piperidine; N-tert-Butylglyoxylsaeureamid; In diethyl ether; at 20 ℃; for 1.5h;

With acetyl chloride; In diethyl ether; at 20 ℃; for 0.333333h;

DOI:10.1021/jo016250v

Reference yield:

C27H39N3O6S*ClH + N-tert-Butylglyoxylsaeureamid (153716-05-3) → C28H40N4O6S

Guidance literature:

With hydrochloric acid 1-ethyl-3-(3-dimethylaminopropyl)carbodiimide hydrochloride; 1-hydroxybenzotriazol-hydrate; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 16h;

Downstream raw materials:

piperidine hydrochloride

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