Technology Process of Crustinic acid
There total 6 articles about Crustinic acid which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogen;
palladium on activated charcoal;
In
ethyl acetate;
for 16h;
DOI:10.1071/C98082
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 90 percent / trifluoroacetic anhydride / toluene / 12 h
2: 90 percent / hydrogen / 10 percent palladium on carbon / ethyl acetate / 16 h
3: 26 percent / potassium hydrogen carbonate, dimethylformamide / 24 h / Ambient temperature
4: 61 percent / trifluoroacetic anhydride / toluene / 12 h
5: 85 percent / hydrogen / 10 percent palladium on carbon / ethyl acetate / 16 h
With
hydrogen; potassium hydrogencarbonate; N,N-dimethyl-formamide; trifluoroacetic anhydride;
palladium on activated charcoal;
In
ethyl acetate; toluene;
DOI:10.1071/C98082
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 9.6 percent / 20 percent aq. sodium hydroxide, potassium persulfate / dioxane / 12 h / Ambient temperature
2: 90 percent / trifluoroacetic anhydride / toluene / 12 h
3: 90 percent / hydrogen / 10 percent palladium on carbon / ethyl acetate / 16 h
4: 26 percent / potassium hydrogen carbonate, dimethylformamide / 24 h / Ambient temperature
5: 61 percent / trifluoroacetic anhydride / toluene / 12 h
6: 85 percent / hydrogen / 10 percent palladium on carbon / ethyl acetate / 16 h
With
sodium hydroxide; potassium peroxomonosulphate; hydrogen; potassium hydrogencarbonate; N,N-dimethyl-formamide; trifluoroacetic anhydride;
palladium on activated charcoal;
In
1,4-dioxane; ethyl acetate; toluene;
DOI:10.1071/C98082
