6-dimethylamino-9-(3-phenylalanylamidobenzyl)-9H-purine dihydrochloride

Base Information

Chemical Name:6-dimethylamino-9-(3-phenylalanylamidobenzyl)-9H-purine dihydrochloride
CAS No.:119805-56-0
Molecular Formula:C₂₃H₂₅N₇O*2ClH
Molecular Weight:488.42
Hs Code.:

Synonyms:6-dimethylamino-9-(3-phenylalanylamidobenzyl)-9H-purine dihydrochloride

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Chemical Property of 6-dimethylamino-9-(3-phenylalanylamidobenzyl)-9H-purine dihydrochloride

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Technology Process of 6-dimethylamino-9-(3-phenylalanylamidobenzyl)-9H-purine dihydrochloride

There total 6 articles about 6-dimethylamino-9-(3-phenylalanylamidobenzyl)-9H-purine dihydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 119805-54-8
9-(3-N-carbobenzoxyphenylalanylamidobenzyl)-6-dimethylamino-9H-purine

: 119805-56-0
6-dimethylamino-9-(3-phenylalanylamidobenzyl)-9H-purine dihydrochloride

Guidance literature:: With hydrogen; palladium on activated charcoal; In acetic acid; for 3.5h; under 1520 - 2280 Torr;
DOI:10.1016/0223-5234(88)90202-4

Reference yield:

: 6952-15-4
6-chloro-9-(3-nitrobenzyl)-9H-purine

: 119805-56-0
6-dimethylamino-9-(3-phenylalanylamidobenzyl)-9H-purine dihydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1: 99 percent / ethanol; H₂O / 17 h / Ambient temperature

2: 94 percent / H₂ / 10percent Pd/C / acetic acid / 1.5 h / 1520 - 2280 Torr

3: 1.) triethylamine, ethyl chloroformate / 1.) THF, 10 min; 2.) THF, r.t., 15 h

4: 92 percent / H₂ / 10percent Pd/C / acetic acid / 3.5 h / 1520 - 2280 Torr

With hydrogen; chloroformic acid ethyl ester; triethylamine; palladium on activated charcoal; In ethanol; water; acetic acid;
DOI:10.1016/0223-5234(88)90202-4

Reference yield:

: 7008-56-2
6-dimethylamino-9-(3-nitrobenzyl)-9H-purine

: 119805-56-0
6-dimethylamino-9-(3-phenylalanylamidobenzyl)-9H-purine dihydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: 94 percent / H₂ / 10percent Pd/C / acetic acid / 1.5 h / 1520 - 2280 Torr

2: 1.) triethylamine, ethyl chloroformate / 1.) THF, 10 min; 2.) THF, r.t., 15 h

3: 92 percent / H₂ / 10percent Pd/C / acetic acid / 3.5 h / 1520 - 2280 Torr

With hydrogen; chloroformic acid ethyl ester; triethylamine; palladium on activated charcoal; In acetic acid;
DOI:10.1016/0223-5234(88)90202-4