DL-[¹³C₆]-4-methoxyamphetamine hydrochloride

Base Information

Chemical Name:DL-[¹³C₆]-4-methoxyamphetamine hydrochloride
CAS No.:1538556-41-0
Molecular Formula:C₁₀H₁₅NO*ClH
Molecular Weight:207.63
Hs Code.:

DL-[<sup>13</sup>C<sub>6</sub>]-4-methoxyamphetamine hydrochloride

Synonyms:DL-[¹³C₆]-4-methoxyamphetamine hydrochloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of DL-[¹³C₆]-4-methoxyamphetamine hydrochloride

Chemical Property:

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Technology Process of DL-[¹³C₆]-4-methoxyamphetamine hydrochloride

There total 3 articles about DL-[¹³C₆]-4-methoxyamphetamine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 1538556-43-2
[¹³C₆]-4-methoxyphenyl-2-propanone

: 1538556-41-0
DL-[¹³C₆]-4-methoxyamphetamine hydrochloride

Guidance literature:: [¹³C₆]-4-methoxyphenyl-2-propanone; With methanol; ammonium acetate; sodium cyanoborohydride; at 22 ℃; Inert atmosphere;

With hydrogenchloride; In diethyl ether; pH=4;
DOI:10.1002/jlcr.3193

Reference yield:

: 152571-52-3,154492-88-3
anisole-1,2,3,4,5,6-¹³C₆

: 1538556-41-0
DL-[¹³C₆]-4-methoxyamphetamine hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1.1: N-Bromosuccinimide / chloroform; N,N-dimethyl-formamide / 70 °C

2.1: tris-(o-tolyl)phosphine; tributyltin methoxide; palladium dichloride / toluene / 4 h / 90 °C / Inert atmosphere

3.1: sodium cyanoborohydride; methanol; ammonium acetate / 22 °C / Inert atmosphere

3.2: pH 4

With methanol; N-Bromosuccinimide; ammonium acetate; tributyltin methoxide; sodium cyanoborohydride; tris-(o-tolyl)phosphine; palladium dichloride; In chloroform; N,N-dimethyl-formamide; toluene;
DOI:10.1002/jlcr.3193

Reference yield:

: 89059-34-7
[¹³C₆]phenol

: 1538556-41-0
DL-[¹³C₆]-4-methoxyamphetamine hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydroxide / water / 0.5 h / Inert atmosphere

1.2: 1 h / 0 - 50 °C / Inert atmosphere

2.1: N-Bromosuccinimide / chloroform; N,N-dimethyl-formamide / 70 °C

3.1: tris-(o-tolyl)phosphine; tributyltin methoxide; palladium dichloride / toluene / 4 h / 90 °C / Inert atmosphere

4.1: sodium cyanoborohydride; methanol; ammonium acetate / 22 °C / Inert atmosphere

4.2: pH 4

With methanol; N-Bromosuccinimide; ammonium acetate; tributyltin methoxide; sodium cyanoborohydride; tris-(o-tolyl)phosphine; sodium hydroxide; palladium dichloride; In chloroform; water; N,N-dimethyl-formamide; toluene;
DOI:10.1002/jlcr.3193