methyl 2-[formyl(4'-methylbiphenyl-4-yl)amino]-4-(6-methyl-4-oxo-1,2,3-benzotriazin-3(4H)-yl)butanoate

Base Information

Chemical Name:methyl 2-[formyl(4'-methylbiphenyl-4-yl)amino]-4-(6-methyl-4-oxo-1,2,3-benzotriazin-3(4H)-yl)butanoate
CAS No.:1369963-02-9
Molecular Formula:C₂₇H₂₆N₄O₄
Molecular Weight:470.528
Hs Code.:

Synonyms:methyl 2-[formyl(4'-methylbiphenyl-4-yl)amino]-4-(6-methyl-4-oxo-1,2,3-benzotriazin-3(4H)-yl)butanoate

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Chemical Property of methyl 2-[formyl(4'-methylbiphenyl-4-yl)amino]-4-(6-methyl-4-oxo-1,2,3-benzotriazin-3(4H)-yl)butanoate

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Technology Process of methyl 2-[formyl(4'-methylbiphenyl-4-yl)amino]-4-(6-methyl-4-oxo-1,2,3-benzotriazin-3(4H)-yl)butanoate

There total 7 articles about methyl 2-[formyl(4'-methylbiphenyl-4-yl)amino]-4-(6-methyl-4-oxo-1,2,3-benzotriazin-3(4H)-yl)butanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 91532-23-9
methyl-6-3H-benzotriazine-1,2,3 one-4

: 1369963-01-8
methyl N-formyl-N-(4'-methylbiphenyl-4-yl)homoserinate

: 1369963-02-9
methyl 2-[formyl(4'-methylbiphenyl-4-yl)amino]-4-(6-methyl-4-oxo-1,2,3-benzotriazin-3(4H)-yl)butanoate

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 0 - 20 ℃; for 0.5h; Inert atmosphere;

Reference yield:

: 5720-05-8
4-methylphenylboronic acid

: 1369963-02-9
methyl 2-[formyl(4'-methylbiphenyl-4-yl)amino]-4-(6-methyl-4-oxo-1,2,3-benzotriazin-3(4H)-yl)butanoate

Guidance literature:: Multi-step reaction with 6 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 3 h / 100 °C / Inert atmosphere

2.1: hydrogen / palladium 10% on activated carbon / tetrahydrofuran; methanol / 2 h / 20 °C

3.1: 3 h / 100 - 110 °C

4.1: toluene / 9 h / Reflux

5.1: sodium hydroxide; water / N,N-dimethyl-formamide / 0.5 h / 20 °C

5.2: 20 °C

6.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 0.5 h / 0 - 20 °C / Inert atmosphere

With di-isopropyl azodicarboxylate; water; hydrogen; potassium carbonate; triphenylphosphine; sodium hydroxide; palladium 10% on activated carbon; In tetrahydrofuran; methanol; N,N-dimethyl-formamide; toluene;

Reference yield:

: 586-78-7
para-nitrophenyl bromide

: 1369963-02-9
methyl 2-[formyl(4'-methylbiphenyl-4-yl)amino]-4-(6-methyl-4-oxo-1,2,3-benzotriazin-3(4H)-yl)butanoate

Guidance literature:: Multi-step reaction with 6 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 3 h / 100 °C / Inert atmosphere

2.1: hydrogen / palladium 10% on activated carbon / tetrahydrofuran; methanol / 2 h / 20 °C

3.1: 3 h / 100 - 110 °C

4.1: toluene / 9 h / Reflux

5.1: sodium hydroxide; water / N,N-dimethyl-formamide / 0.5 h / 20 °C

5.2: 20 °C

6.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 0.5 h / 0 - 20 °C / Inert atmosphere

With di-isopropyl azodicarboxylate; water; hydrogen; potassium carbonate; triphenylphosphine; sodium hydroxide; palladium 10% on activated carbon; In tetrahydrofuran; methanol; N,N-dimethyl-formamide; toluene;