1-benzyl-N-(diaminomethylene)-3-[(dimethylamino)methyl]-1H-indole-5-carboxamide

Base Information

Chemical Name:1-benzyl-N-(diaminomethylene)-3-[(dimethylamino)methyl]-1H-indole-5-carboxamide
CAS No.:947413-24-3
Molecular Formula:C₂₀H₂₃N₅O
Molecular Weight:349.436
Hs Code.:

Synonyms:1-benzyl-N-(diaminomethylene)-3-[(dimethylamino)methyl]-1H-indole-5-carboxamide

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Chemical Property of 1-benzyl-N-(diaminomethylene)-3-[(dimethylamino)methyl]-1H-indole-5-carboxamide

Chemical Property:

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Technology Process of 1-benzyl-N-(diaminomethylene)-3-[(dimethylamino)methyl]-1H-indole-5-carboxamide

There total 3 articles about 1-benzyl-N-(diaminomethylene)-3-[(dimethylamino)methyl]-1H-indole-5-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₉H₂₀N₂O₂

: 593-85-1,90332-86-8,3425-08-9
diguanidine carbonate

: 947413-24-3
1-benzyl-N-(diaminomethylene)-3-[(dimethylamino)methyl]-1H-indole-5-carboxamide

Guidance literature:: C₁₉H₂₀N₂O₂; With 1,1'-carbonyldiimidazole; In N,N-dimethyl-formamide; at 50 ℃; for 1h;

diguanidine carbonate; In N,N-dimethyl-formamide; at 20 ℃;

Reference yield:

: 197506-83-5
methyl 3‐formyl‐1H‐indole‐5‐carboxylate

: 947413-24-3
1-benzyl-N-(diaminomethylene)-3-[(dimethylamino)methyl]-1H-indole-5-carboxamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydroxide; acetic acid; triethylamine / dichloromethane / 1 h / 20 °C

1.2: 0 - 20 °C

1.3: 0 °C / pH 8

2.1: sodium hydroxide; ethanol; water / 80 °C

2.2: 0 °C

3.1: 1,1'-carbonyldiimidazole / N,N-dimethyl-formamide / 1 h / 50 °C

3.2: 20 °C

With sodium hydroxide; ethanol; water; acetic acid; triethylamine; 1,1'-carbonyldiimidazole; In dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 947413-03-8
methyl 1-benzyl-3-[(dimethylamino)methyl]-1H-indole-5-carboxylate

: 947413-24-3
1-benzyl-N-(diaminomethylene)-3-[(dimethylamino)methyl]-1H-indole-5-carboxamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydroxide; ethanol; water / 80 °C

1.2: 0 °C

2.1: 1,1'-carbonyldiimidazole / N,N-dimethyl-formamide / 1 h / 50 °C

2.2: 20 °C

With sodium hydroxide; ethanol; water; 1,1'-carbonyldiimidazole; In N,N-dimethyl-formamide;