4-amino-3-<3,5-dimethyl-1-(4-nitrophenyl)-1H-pyrazol-4-yl>methylene-1,2,4-triazole-5-thiol

Base Information

• Chemical Name: 4-amino-3-<3,5-dimethyl-1-(4-nitrophenyl)-1H-pyrazol-4-yl>methylene-1,2,4-triazole-5-thiol
• CAS No.: 127871-88-9
• Molecular Formula: C₁₄H₁₅N₇O₂S
• Molecular Weight: 345.385

Synonyms:4-amino-3-<3,5-dimethyl-1-(4-nitrophenyl)-1H-pyrazol-4-yl>methylene-1,2,4-triazole-5-thiol

Chemical Property of 4-amino-3-<3,5-dimethyl-1-(4-nitrophenyl)-1H-pyrazol-4-yl>methylene-1,2,4-triazole-5-thiol

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Technology Process of 4-amino-3-<3,5-dimethyl-1-(4-nitrophenyl)-1H-pyrazol-4-yl>methylene-1,2,4-triazole-5-thiol

There total 6 articles about 4-amino-3-<3,5-dimethyl-1-(4-nitrophenyl)-1H-pyrazol-4-yl>methylene-1,2,4-triazole-5-thiol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

C14H14N5O3S2(1-)*K(1+) (127871-87-8) → 4-amino-3-<3,5-dimethyl-1-(4-nitrophenyl)-1H-pyrazol-4-yl>methylene-1,2,4-triazole-5-thiol (127871-88-9)

Guidance literature:

With hydrazine hydrate; In water; for 1h; Heating;

Reference yield: 15.0%

Thiobenzoic acid S-{5-[3,5-dimethyl-1-(4-nitro-phenyl)-1H-pyrazol-4-ylmethyl]-[1,3,4]thiadiazol-2-yl} ester (127872-02-0) → {5-[3,5-Dimethyl-1-(4-nitro-phenyl)-1H-pyrazol-4-ylmethyl]-[1,3,4]thiadiazol-2-yl}-hydrazine (127872-03-1) + 4-amino-3-<3,5-dimethyl-1-(4-nitrophenyl)-1H-pyrazol-4-yl>methylene-1,2,4-triazole-5-thiol (127871-88-9)

Guidance literature:

With hydrazine hydrate; In ethanol; for 82h; Ambient temperature;

Reference yield: 15.0%

Thioacetic acid S-{5-[3,5-dimethyl-1-(4-nitro-phenyl)-1H-pyrazol-4-ylmethyl]-[1,3,4]thiadiazol-2-yl} ester (127872-01-9) → {5-[3,5-Dimethyl-1-(4-nitro-phenyl)-1H-pyrazol-4-ylmethyl]-[1,3,4]thiadiazol-2-yl}-hydrazine (127872-03-1) + 4-amino-3-<3,5-dimethyl-1-(4-nitrophenyl)-1H-pyrazol-4-yl>methylene-1,2,4-triazole-5-thiol (127871-88-9)

Guidance literature:

With hydrazine hydrate; In ethanol; for 82h; Ambient temperature;

upstream raw materials:

2-<3,5-dimethyl-1-(4-nitrophenyl)-1H-pyrazol-4-yl>methylene-1,3,4-thiadiazole-5-thiol

Thioacetic acid S-{5-[3,5-dimethyl-1-(4-nitro-phenyl)-1H-pyrazol-4-ylmethyl]-[1,3,4]thiadiazol-2-yl} ester

Thiobenzoic acid S-{5-[3,5-dimethyl-1-(4-nitro-phenyl)-1H-pyrazol-4-ylmethyl]-[1,3,4]thiadiazol-2-yl} ester

C₁₄H₁₄N₅O₃S₂^(1-)*K⁽¹⁺⁾

Downstream raw materials:

3-[3,5-Dimethyl-1-(4-nitro-phenyl)-1H-pyrazol-4-ylmethyl]-[1,2,4]triazolo[3,4-b][1,3,4]thiadiazole-6-thiol

3-[3,5-Dimethyl-1-(4-nitro-phenyl)-1H-pyrazol-4-ylmethyl]-[1,2,4]triazolo[3,4-b][1,3,4]thiadiazol-6-ol

3-[3,5-Dimethyl-1-(4-nitro-phenyl)-1H-pyrazol-4-ylmethyl]-[1,2,4]triazolo[3,4-b][1,3,4]thiadiazole

3-[3,5-Dimethyl-1-(4-nitro-phenyl)-1H-pyrazol-4-ylmethyl]-6-methyl-[1,2,4]triazolo[3,4-b][1,3,4]thiadiazole

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