1-deoxy-4,6-O-benzylidene-3-O-methyl-5-C-hydroxymethyl-1-phenyl-sulfinyl-β-D-glucopyranoside

Base Information

Chemical Name:1-deoxy-4,6-O-benzylidene-3-O-methyl-5-C-hydroxymethyl-1-phenyl-sulfinyl-β-D-glucopyranoside
CAS No.:1352407-00-1
Molecular Formula:C₂₁H₂₄O₇S
Molecular Weight:420.483
Hs Code.:

Synonyms:1-deoxy-4,6-O-benzylidene-3-O-methyl-5-C-hydroxymethyl-1-phenyl-sulfinyl-β-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-deoxy-4,6-O-benzylidene-3-O-methyl-5-C-hydroxymethyl-1-phenyl-sulfinyl-β-D-glucopyranoside

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Technology Process of 1-deoxy-4,6-O-benzylidene-3-O-methyl-5-C-hydroxymethyl-1-phenyl-sulfinyl-β-D-glucopyranoside

There total 5 articles about 1-deoxy-4,6-O-benzylidene-3-O-methyl-5-C-hydroxymethyl-1-phenyl-sulfinyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₁H₂₂O₆S

: 1352407-00-1
1-deoxy-4,6-O-benzylidene-3-O-methyl-5-C-hydroxymethyl-1-phenyl-sulfinyl-β-D-glucopyranoside

Guidance literature:: With sodium tetrahydroborate; In methanol; at 20 ℃; for 2h;
DOI:10.1016/j.bmcl.2011.10.005

Reference yield:

: 1352406-92-8
phenyl 4,6-O-benzylidene-3-O-methyl-5-C-vinyl-1-thio-β-D-glucopyranoside

: 1352407-00-1
1-deoxy-4,6-O-benzylidene-3-O-methyl-5-C-hydroxymethyl-1-phenyl-sulfinyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: ozone / dichloromethane / 0.05 h / -78 °C

2: sodium tetrahydroborate / ethanol / 2 h / 0 - 20 °C

With sodium tetrahydroborate; ozone; In ethanol; dichloromethane;
DOI:10.1016/j.bmcl.2011.10.005

Reference yield:

: C₁₅H₂₀O₅S

: 1352407-00-1
1-deoxy-4,6-O-benzylidene-3-O-methyl-5-C-hydroxymethyl-1-phenyl-sulfinyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: toluene-4-sulfonic acid / N,N-dimethyl-formamide / 3 h / 70 °C / Inert atmosphere

2: ozone / dichloromethane / 0.05 h / -78 °C

3: sodium tetrahydroborate / ethanol / 2 h / 0 - 20 °C

With sodium tetrahydroborate; toluene-4-sulfonic acid; ozone; In ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.10.005