benzyl 4-[3-(tetra-O-acetyl-β-d-glucopyranosyloxy)-5-isopropyl-1H-pyrazol-4-ylmethyl]benzoate

Base Information

Chemical Name:benzyl 4-[3-(tetra-O-acetyl-β-d-glucopyranosyloxy)-5-isopropyl-1H-pyrazol-4-ylmethyl]benzoate
CAS No.:1422008-45-4
Molecular Formula:C₃₅H₄₀N₂O₁₂
Molecular Weight:680.709
Hs Code.:

Synonyms:benzyl 4-[3-(tetra-O-acetyl-β-d-glucopyranosyloxy)-5-isopropyl-1H-pyrazol-4-ylmethyl]benzoate

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Chemical Property of benzyl 4-[3-(tetra-O-acetyl-β-d-glucopyranosyloxy)-5-isopropyl-1H-pyrazol-4-ylmethyl]benzoate

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Technology Process of benzyl 4-[3-(tetra-O-acetyl-β-d-glucopyranosyloxy)-5-isopropyl-1H-pyrazol-4-ylmethyl]benzoate

There total 3 articles about benzyl 4-[3-(tetra-O-acetyl-β-d-glucopyranosyloxy)-5-isopropyl-1H-pyrazol-4-ylmethyl]benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

: 572-09-8,3068-32-4,4026-32-8,6919-96-6,13242-53-0,14227-54-4,14795-18-7,19186-59-5,19285-38-2,21698-13-5,29907-26-4,53369-42-9,60619-58-1,61303-35-3,67337-79-5,69127-37-3,70749-15-4,72002-90-5,75247-30-2,75880-74-9,78418-57-2,102339-89-9,102339-90-2,103530-40-1,114028-03-4,114718-45-5,138514-70-2,138514-71-3
2,3,4,6-tetra-O-acetyl-D-glucopyranosyl bromide

: 1422008-38-5
benzyl 4-(1,2-dihydro-3-oxo-5-isopropyl-3H-pyrazol-4-ylmethyl)benzoate

: 1422008-45-4
benzyl 4-[3-(tetra-O-acetyl-β-d-glucopyranosyloxy)-5-isopropyl-1H-pyrazol-4-ylmethyl]benzoate

Guidance literature:: With benzyltri(n-butyl)ammonium chloride; sodium hydroxide; In dichloromethane; at 20 ℃;
DOI:10.1016/j.bmc.2012.11.041

Reference yield:

: 1034494-08-0
4-methanesulfonyloxymethylbenzoic acid benzyl ester

: 1422008-45-4
benzyl 4-[3-(tetra-O-acetyl-β-d-glucopyranosyloxy)-5-isopropyl-1H-pyrazol-4-ylmethyl]benzoate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydride / tetrahydrofuran / 10 h / 0 °C / Reflux

2: hydrazine hydrate / isopropyl alcohol / 20 °C

3: benzyltri(n-butyl)ammonium chloride; sodium hydroxide / dichloromethane / 20 °C

With benzyltri(n-butyl)ammonium chloride; sodium hydride; hydrazine hydrate; sodium hydroxide; In tetrahydrofuran; dichloromethane; isopropyl alcohol;
DOI:10.1016/j.bmc.2012.11.041

Reference yield:

: 3006-96-0
3-hydroxymethyl-benzoic acid

: 1422008-45-4
benzyl 4-[3-(tetra-O-acetyl-β-d-glucopyranosyloxy)-5-isopropyl-1H-pyrazol-4-ylmethyl]benzoate

Guidance literature:: Multi-step reaction with 5 steps

1: potassium carbonate / N,N-dimethyl-formamide / 20 °C

2: triethylamine / tetrahydrofuran / 0.33 h / 0 °C

3: sodium hydride / tetrahydrofuran / 10 h / 0 °C / Reflux

4: hydrazine hydrate / isopropyl alcohol / 20 °C

5: benzyltri(n-butyl)ammonium chloride; sodium hydroxide / dichloromethane / 20 °C

With benzyltri(n-butyl)ammonium chloride; sodium hydride; potassium carbonate; hydrazine hydrate; triethylamine; sodium hydroxide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; isopropyl alcohol;
DOI:10.1016/j.bmc.2012.11.041