[GeCl{GeCl(mesityl)2}(1,3-diisopropyl-4,5-dimethylimidazol-2-ylidene)]

Base Information

Chemical Name:[GeCl{GeCl(mesityl)2}(1,3-diisopropyl-4,5-dimethylimidazol-2-ylidene)]
CAS No.:1067499-18-6
Molecular Formula:C₂₉H₄₂Cl₂Ge₂N₂
Molecular Weight:634.752
Hs Code.:

Synonyms:[GeCl{GeCl(mesityl)2}(1,3-diisopropyl-4,5-dimethylimidazol-2-ylidene)]

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Chemical Property of [GeCl{GeCl(mesityl)2}(1,3-diisopropyl-4,5-dimethylimidazol-2-ylidene)]

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Technology Process of [GeCl{GeCl(mesityl)2}(1,3-diisopropyl-4,5-dimethylimidazol-2-ylidene)]

There total 2 articles about [GeCl{GeCl(mesityl)2}(1,3-diisopropyl-4,5-dimethylimidazol-2-ylidene)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 28595-67-7
GeCl₂(1,4-dioxane)

: C₂₉H₄₂Ge₂N₂

: 1067499-18-6
[GeCl{GeCl(mesityl)2}(1,3-diisopropyl-4,5-dimethylimidazol-2-ylidene)]

Guidance literature:: In tetrahydrofuran; at 50 ℃; for 48h; Inert atmosphere; Schlenk technique;
DOI:10.1246/cl.2013.43

Reference yield: 25.0%

: (1,3-diisoproyl-4,5-dimethylimidazolin-2-ylidene)bis(2,4,6-trimethylphenyl)germanium(II)

: 1000619-32-8
dichloro(1,3-diisopropyl-4,5-dimethylimidazolin-2-ylidene)germanium(II)

: 1067499-18-6
[GeCl{GeCl(mesityl)2}(1,3-diisopropyl-4,5-dimethylimidazol-2-ylidene)]

Guidance literature:: In tetrahydrofuran; under N2; soln. of GeCl2 complex added to soln. of Ge-dimesityl complex in THF; stirred for 2 d; solvent removed under vac.; suspended in benzene; centrifuged; pentane added to soln.; ppt. collected; triturated with pentane; dried under vac.; elem. anal.;
DOI:10.1021/om800368d