N-[2-(6-methoxy-1-methyl-9H-carbazol-2-yl)ethyl]terephthalamic acid methyl ester

Base Information

Chemical Name:N-[2-(6-methoxy-1-methyl-9H-carbazol-2-yl)ethyl]terephthalamic acid methyl ester
CAS No.:1262748-76-4
Molecular Formula:C₂₅H₂₄N₂O₄
Molecular Weight:416.477
Hs Code.:

Synonyms:N-[2-(6-methoxy-1-methyl-9H-carbazol-2-yl)ethyl]terephthalamic acid methyl ester

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Chemical Property of N-[2-(6-methoxy-1-methyl-9H-carbazol-2-yl)ethyl]terephthalamic acid methyl ester

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Technology Process of N-[2-(6-methoxy-1-methyl-9H-carbazol-2-yl)ethyl]terephthalamic acid methyl ester

There total 1 articles about N-[2-(6-methoxy-1-methyl-9H-carbazol-2-yl)ethyl]terephthalamic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 1679-64-7
Monomethyl terephthalate

: 95835-25-9
2-(6-methoxy-1-methyl-9H-carbazol-2-yl)ethylamine

: 1262748-76-4
N-[2-(6-methoxy-1-methyl-9H-carbazol-2-yl)ethyl]terephthalamic acid methyl ester

Guidance literature:: Monomethyl terephthalate; With chloroformic acid ethyl ester; triethylamine; In tetrahydrofuran; at -10 ℃; for 0.5h;

2-(6-methoxy-1-methyl-9H-carbazol-2-yl)ethylamine; In tetrahydrofuran; at -10 - 20 ℃; for 24h;

Reference yield: 48.0%

: 1262748-76-4
N-[2-(6-methoxy-1-methyl-9H-carbazol-2-yl)ethyl]terephthalamic acid methyl ester

: 1262748-78-6
9-methoxy-5-methyl-1-(4-methoxycarbonylphenyl)-3,4-dihydro-6H-pyrido[4,3-b]carbazole

Guidance literature:: With trichlorophosphate; In toluene; for 5h; Reflux;

Reference yield:

: 1262748-76-4
N-[2-(6-methoxy-1-methyl-9H-carbazol-2-yl)ethyl]terephthalamic acid methyl ester

: 1262748-80-0
9-methoxy-5-methyl-1-(4-methoxycarbonylphenyl)-6H-pyrido[4,3-b]carbazole

Guidance literature:: Multi-step reaction with 2 steps

1: trichlorophosphate / toluene / 5 h / Reflux

2: palladium 10% on activated carbon / diphenylether / 0.5 h / Reflux

With palladium 10% on activated carbon; trichlorophosphate; In diphenylether; toluene;