(1R,2R,5S)-methyl 2-benzyloxycarbonylamino-5-t-butoxycarbonylaminocyclohex-3-enecarboxylic acid

Base Information

Chemical Name:(1R,2R,5S)-methyl 2-benzyloxycarbonylamino-5-t-butoxycarbonylaminocyclohex-3-enecarboxylic acid
CAS No.:581100-15-4
Molecular Formula:C₂₀H₂₆N₂O₆
Molecular Weight:390.436
Hs Code.:

Synonyms:(1R,2R,5S)-methyl 2-benzyloxycarbonylamino-5-t-butoxycarbonylaminocyclohex-3-enecarboxylic acid

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Chemical Property of (1R,2R,5S)-methyl 2-benzyloxycarbonylamino-5-t-butoxycarbonylaminocyclohex-3-enecarboxylic acid

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Technology Process of (1R,2R,5S)-methyl 2-benzyloxycarbonylamino-5-t-butoxycarbonylaminocyclohex-3-enecarboxylic acid

There total 1 articles about (1R,2R,5S)-methyl 2-benzyloxycarbonylamino-5-t-butoxycarbonylaminocyclohex-3-enecarboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 581100-14-3
(1R,2R,5S)-methyl 2-benzyloxycarbonylamino-5-t-butoxycarbonylaminocyclohex-3-enecarboxylate

: 581100-15-4
(1R,2R,5S)-methyl 2-benzyloxycarbonylamino-5-t-butoxycarbonylaminocyclohex-3-enecarboxylic acid

Guidance literature:: (1R,2R,5S)-methyl 2-benzyloxycarbonylamino-5-t-butoxycarbonylaminocyclohex-3-enecarboxylate; With sodium hydroxide; In methanol; dichloromethane; at 0 - 20 ℃; for 16h;

With hydrogenchloride; In methanol; dichloromethane;

Reference yield: 77.0%

: 581100-15-4
(1R,2R,5S)-methyl 2-benzyloxycarbonylamino-5-t-butoxycarbonylaminocyclohex-3-enecarboxylic acid

: 2916-68-9
2-(Trimethylsilyl)ethanol

: 581100-16-5
(1R,2R,5S)-2-Benzyloxycarbonylamino-5-t-butoxycarbonylamino-1-(2-trimethylsilyl)ethoxycarbonylaminocyclohex-3-ene

Guidance literature:: (1R,2R,5S)-methyl 2-benzyloxycarbonylamino-5-t-butoxycarbonylaminocyclohex-3-enecarboxylic acid; With chloroformic acid ethyl ester; triethylamine; In tetrahydrofuran; at 0 ℃; for 1h;

With sodium azide; In tetrahydrofuran; water; at 0 ℃; for 2h;

2-(Trimethylsilyl)ethanol; In benzene; for 3h; Reflux;