(3aR,5R,6S,6aR)-6-Benzyloxy-5-dodecyl-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxole

Base Information

Chemical Name:(3aR,5R,6S,6aR)-6-Benzyloxy-5-dodecyl-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxole
CAS No.:213455-93-7
Molecular Formula:C₂₆H₄₂O₄
Molecular Weight:418.617
Hs Code.:

Synonyms:(3aR,5R,6S,6aR)-6-Benzyloxy-5-dodecyl-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxole

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Chemical Property of (3aR,5R,6S,6aR)-6-Benzyloxy-5-dodecyl-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxole

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Technology Process of (3aR,5R,6S,6aR)-6-Benzyloxy-5-dodecyl-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxole

There total 1 articles about (3aR,5R,6S,6aR)-6-Benzyloxy-5-dodecyl-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-44-7
benzyl chloride

: (3aR,5R,6S,6aR)-5-Dodecyl-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-ol

: 213455-93-7
(3aR,5R,6S,6aR)-6-Benzyloxy-5-dodecyl-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxole

Guidance literature:: With sodium hydride; Yield given. Multistep reaction; 1.) DMSO, THF, room temperature, 30 min, 2.) room temperature, 5 h;
DOI:10.1016/S0968-0896(98)00062-5

Reference yield: 67.0%

: 213455-93-7
(3aR,5R,6S,6aR)-6-Benzyloxy-5-dodecyl-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxole

: 213455-70-0
(2S,3R,4R,5R)-4-Benzyloxy-5-dodecyl-tetrahydro-furan-2,3-diol

Guidance literature:: With hydrogenchloride; In 1,2-dimethoxyethane; for 48h; Ambient temperature;
DOI:10.1016/S0968-0896(98)00062-5

Reference yield:

: 213455-93-7
(3aR,5R,6S,6aR)-6-Benzyloxy-5-dodecyl-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxole

: (4R,5R)-4-Benzyloxy-5-hydroxy-heptadecanoic acid ethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 67 percent / HCl / 1,2-dimethoxy-ethane / 48 h / Ambient temperature

2: 73 percent / NaIO₄ / methanol / 1 h / Ambient temperature

3: 1.) NaH / 1.) THF, 0 deg C, 30 min, 2.) THF, room temperature, 3 h

4: H₂ / Pd/C / ethyl acetate / 24 h / Ambient temperature

With hydrogenchloride; sodium periodate; hydrogen; sodium hydride; palladium on activated charcoal; In methanol; 1,2-dimethoxyethane; ethyl acetate;
DOI:10.1016/S0968-0896(98)00062-5