1,2-Dichloro-4-trifluoromethylsulfanylmethylsulfanyl-benzene

Base Information

• Chemical Name: 1,2-Dichloro-4-trifluoromethylsulfanylmethylsulfanyl-benzene
• CAS No.: 204908-55-4
• Molecular Formula: C₈H₅Cl₂F₃S₂
• Molecular Weight: 293.161
• Mol file: 204908-55-4.mol

Synonyms:1,2-Dichloro-4-trifluoromethylsulfanylmethylsulfanyl-benzene

Chemical Property of 1,2-Dichloro-4-trifluoromethylsulfanylmethylsulfanyl-benzene

Chemical Property:

Purity/Quality:

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MSDS Files:

Useful:

Technology Process of 1,2-Dichloro-4-trifluoromethylsulfanylmethylsulfanyl-benzene

There total 1 articles about 1,2-Dichloro-4-trifluoromethylsulfanylmethylsulfanyl-benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

chloromethyl-trifluoromethyl sulfide (460-58-2) + 3,4-dichlorothiophenol (5858-17-3) → 1,2-Dichloro-4-trifluoromethylsulfanylmethylsulfanyl-benzene (204908-55-4)

Guidance literature:

With sodium methylate; Yield given. Multistep reaction; 1.) MeOH, 30 min, 2.) MeOH, reflux, 18 h;

DOI:10.1021/jm970678y

Reference yield: 65.0%

1,2-Dichloro-4-trifluoromethylsulfanylmethylsulfanyl-benzene (204908-55-4) → 1,2-Dichloro-4-trifluoromethylsulfanylmethanesulfonyl-benzene (204908-56-5)

Guidance literature:

With dihydrogen peroxide; acetic acid; 1.) RT, 2 h, 2.) 65 deg C, 2 h;

DOI:10.1021/jm970678y

Reference yield:

1,2-Dichloro-4-trifluoromethylsulfanylmethylsulfanyl-benzene (204908-55-4) → [(3,4-dichlorophenyl)sulfonyl][(trifluoromethyl)sulfonyl]methane

Guidance literature:

With dihydrogen peroxide; trifluoroacetic acid; 1.) RT, overnight, 2.) 70 deg C, 8 h;

DOI:10.1021/jm970678y

upstream raw materials:

chloromethyl-trifluoromethyl sulfide

3,4-dichlorothiophenol

Downstream raw materials:

1,2-Dichloro-4-trifluoromethylsulfanylmethanesulfonyl-benzene