3β-hydroxy-5α-androstan-16-ylidene-[(sulfanyl)methyl-(2'-oxo-2'-phenylimino-N-(p-methylphenyl)ethanhydrazonothioate)]-17one

Base Information

Chemical Name:3β-hydroxy-5α-androstan-16-ylidene-[(sulfanyl)methyl-(2'-oxo-2'-phenylimino-N-(p-methylphenyl)ethanhydrazonothioate)]-17one
CAS No.:1241792-28-8
Molecular Formula:C₃₅H₄₃N₃O₃S₂
Molecular Weight:617.877
Hs Code.:

Synonyms:3β-hydroxy-5α-androstan-16-ylidene-[(sulfanyl)methyl-(2'-oxo-2'-phenylimino-N-(p-methylphenyl)ethanhydrazonothioate)]-17one

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Chemical Property of 3β-hydroxy-5α-androstan-16-ylidene-[(sulfanyl)methyl-(2'-oxo-2'-phenylimino-N-(p-methylphenyl)ethanhydrazonothioate)]-17one

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Technology Process of 3β-hydroxy-5α-androstan-16-ylidene-[(sulfanyl)methyl-(2'-oxo-2'-phenylimino-N-(p-methylphenyl)ethanhydrazonothioate)]-17one

There total 1 articles about 3β-hydroxy-5α-androstan-16-ylidene-[(sulfanyl)methyl-(2'-oxo-2'-phenylimino-N-(p-methylphenyl)ethanhydrazonothioate)]-17one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 75-15-0,12122-00-8
carbon disulfide

: 481-29-8
Epiandrosterone

: 33101-95-0,132815-68-0
2-anilino-N-(4-methylphenyl)-2-oxoethanehydrazonoyl chloride

: 1241792-28-8
3β-hydroxy-5α-androstan-16-ylidene-[(sulfanyl)methyl-(2'-oxo-2'-phenylimino-N-(p-methylphenyl)ethanhydrazonothioate)]-17one

Guidance literature:: carbon disulfide; Epiandrosterone; With sodium hydride; In dimethyl sulfoxide; mineral oil; at 0 ℃; for 3h; Inert atmosphere;

2-anilino-N-(4-methylphenyl)-2-oxoethanehydrazonoyl chloride; In dimethyl sulfoxide; mineral oil; at 0 ℃; Inert atmosphere;
DOI:10.1080/10426500903008914