C₁₄H₂₂O₃

Base Information

Chemical Name:C₁₄H₂₂O₃
CAS No.:945426-73-3
Molecular Formula:C₁₄H₂₂O₃
Molecular Weight:238.327
Hs Code.:

C<sub>14</sub>H<sub>22</sub>O<sub>3</sub>

Synonyms:C₁₄H₂₂O₃

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Chemical Property of C₁₄H₂₂O₃

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Technology Process of C₁₄H₂₂O₃

There total 6 articles about C₁₄H₂₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 945426-72-2
C₁₄H₂₄O₃

: 945426-73-3
C₁₄H₂₂O₃

Guidance literature:: With pyridinium chlorochromate; In dichloromethane; at 20 ℃; for 4h;
DOI:10.1080/00397910701196546

Reference yield:

: 945426-65-3
4-(2,6,6-trimethyl-2-cyclohexen-1-ylidene)-2-methoxybutane

: 945426-73-3
C₁₄H₂₂O₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: anhydrous sodium carbonate; m-chloroperbenzoic acid / CH₂Cl₂ / 8 h / 20 °C

1.2: 200 mg / sulfuric acid / H₂O; diethyl ether / 6 h / 20 °C

2.1: sodium carbonate; m-chloroperbenzoic acid / CH₂Cl₂ / 7 h / 20 °C

3.1: 551 mg / active neutral alumina / diethyl ether / 12 h / 20 °C

4.1: 86 percent / pyridinium chlorochromate / CH₂Cl₂ / 4 h / 20 °C

With aluminum oxide; sodium carbonate; 3-chloro-benzenecarboperoxoic acid; pyridinium chlorochromate; In diethyl ether; dichloromethane;
DOI:10.1080/00397910701196546

Reference yield:

: C₁₄H₂₄O₃

: 945426-73-3
C₁₄H₂₂O₃

Guidance literature:: Multi-step reaction with 2 steps

1: 551 mg / active neutral alumina / diethyl ether / 12 h / 20 °C

2: 86 percent / pyridinium chlorochromate / CH₂Cl₂ / 4 h / 20 °C

With aluminum oxide; pyridinium chlorochromate; In diethyl ether; dichloromethane;
DOI:10.1080/00397910701196546