2-(tert-butyl)-4-(1-(5-(tert-butyl)-3-(chloromethyl)-4-hydroxyphenyl)isopropyl)-6-(chloromethyl)phenol

Base Information

• Chemical Name: 2-(tert-butyl)-4-(1-(5-(tert-butyl)-3-(chloromethyl)-4-hydroxyphenyl)isopropyl)-6-(chloromethyl)phenol
• CAS No.: 333334-76-2
• Molecular Formula: C₂₅H₃₄Cl₂O₂
• Molecular Weight: 437.45

Synonyms:2-(tert-butyl)-4-(1-(5-(tert-butyl)-3-(chloromethyl)-4-hydroxyphenyl)isopropyl)-6-(chloromethyl)phenol

Chemical Property of 2-(tert-butyl)-4-(1-(5-(tert-butyl)-3-(chloromethyl)-4-hydroxyphenyl)isopropyl)-6-(chloromethyl)phenol

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Technology Process of 2-(tert-butyl)-4-(1-(5-(tert-butyl)-3-(chloromethyl)-4-hydroxyphenyl)isopropyl)-6-(chloromethyl)phenol

There total 2 articles about 2-(tert-butyl)-4-(1-(5-(tert-butyl)-3-(chloromethyl)-4-hydroxyphenyl)isopropyl)-6-(chloromethyl)phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

6-(tert-butyl)-4-(1-(5-(tert-butyl)-4-hydroxy-3-(hydroxymethyl)phenyl)isopropyl)-2-(hydroxymethyl)phenol (122041-35-4) → 2-(tert-butyl)-4-(1-(5-(tert-butyl)-3-(chloromethyl)-4-hydroxyphenyl)isopropyl)-6-(chloromethyl)phenol (333334-76-2)

Guidance literature:

With thionyl chloride; In benzene; at 20 ℃; for 3h;

DOI:10.1002/jhet.5570370612

Reference yield:

2,2'-di-tert-butyl-4,4'-(propane-2,2-diyl)diphenol (79-96-9) → 2-(tert-butyl)-4-(1-(5-(tert-butyl)-3-(chloromethyl)-4-hydroxyphenyl)isopropyl)-6-(chloromethyl)phenol (333334-76-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 55 percent / 20 percent aq. KOH / methanol / 1.5 h / 45 °C

2: 90 percent / thionyl chloride / benzene / 3 h / 20 °C

With potassium hydroxide; thionyl chloride; In methanol; benzene;

DOI:10.1002/jhet.5570370612

Reference yield: 50.0%

(R)-1-phenyl-ethyl-amine (3886-69-9) + 2-(tert-butyl)-4-(1-(5-(tert-butyl)-3-(chloromethyl)-4-hydroxyphenyl)isopropyl)-6-(chloromethyl)phenol (333334-76-2) → 9,23-diaza-9,23-bis((1R)-1-phenylethyl)-2,2,16,16-tetramethyl-5,13,19,27-tetrakis(tert-butyl)-pentacyclo[23.3.1.13,7.111,15.117,21]dotriaconta-1(28),3(4),5,7(30),11(12),13,15(31),17(18),19,21(32),25(29),26-dodecaene-6,12,20,26-tetraol

Guidance literature:

With sodium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 5h;

DOI:10.1002/jhet.5570370612

upstream raw materials:

6-(tert-butyl)-4-(1-(5-(tert-butyl)-4-hydroxy-3-(hydroxymethyl)phenyl)isopropyl)-2-(hydroxymethyl)phenol

2,2'-di-tert-butyl-4,4'-(propane-2,2-diyl)diphenol

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