C₆₂H₁₁₂O₁₁Si₃

Base Information

Chemical Name:C₆₂H₁₁₂O₁₁Si₃
CAS No.:175612-30-3
Molecular Formula:C₆₂H₁₁₂O₁₁Si₃
Molecular Weight:1117.82
Hs Code.:

C<sub>62</sub>H<sub>112</sub>O<sub>11</sub>Si<sub>3</sub>

Synonyms:C₆₂H₁₁₂O₁₁Si₃

Suppliers and Price of C₆₂H₁₁₂O₁₁Si₃

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₆₂H₁₁₂O₁₁Si₃

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₆₂H₁₁₂O₁₁Si₃

There total 40 articles about C₆₂H₁₁₂O₁₁Si₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: C₆₅H₁₁₈O₁₀S₂Si₃

: 175612-30-3
C₆₂H₁₁₂O₁₁Si₃

Guidance literature:: With N-Bromosuccinimide; silver perchlorate; In water; acetone; at 0 ℃; for 0.00833333h;

Reference yield:

: 59983-36-7
(S)-1-(1-Ethylpropylidenamino)-2-methoxymethylpyrrolidin

: 175612-30-3
C₆₂H₁₁₂O₁₁Si₃

Guidance literature:: Multi-step reaction with 10 steps

1: 1.) LDA / 1.) Et₂O, hexane, 0 deg C, 4 h, 2.) Et₂O, hexane, from -110 deg C to RT, 12 h

2: 97 percent / O₃ / CH₂Cl₂ / -78 °C

3: 1.) TiCl₄, Et₃N / 1.) CH₂Cl₂, -78 deg C, 2.5 h, 2.) CH₂Cl₂, -78 deg C, 2.5 h

4: 89 percent / SmI₂ / tetrahydrofuran / 1 h / -10 °C

5: 86 percent / 2,6-lutidine / CH₂Cl₂ / 1 h / 0 - 20 °C

6: 99 percent / H₂ / 10percent Pd/C / ethanol / 48 h / Ambient temperature

7: Et₃N, SOCl₂ / CH₂Cl₂ / 0.17 h / 0 °C

8: RuCl₃, NaIO₄ / CCl₄; acetonitrile; H₂O / 1.5 h / 0 °C

9: 1.) t-BuLi, HMPA, 3.) 30percent aq. H₂SO₄

10: 91 percent / NBS, AgClO₄ / acetone; H₂O / 0.01 h / 0 °C

With 2,6-dimethylpyridine; N,N,N,N,N,N-hexamethylphosphoric triamide; ruthenium trichloride; sodium periodate; N-Bromosuccinimide; thionyl chloride; samarium diiodide; sulfuric acid; hydrogen; tert.-butyl lithium; silver perchlorate; titanium tetrachloride; ozone; triethylamine; lithium diisopropyl amide; palladium on activated charcoal; In tetrahydrofuran; tetrachloromethane; ethanol; dichloromethane; water; acetone; acetonitrile;

Reference yield:

: 73-34-7
L-rhamnose

: 175612-30-3
C₆₂H₁₁₂O₁₁Si₃

Guidance literature:: Multi-step reaction with 18 steps

1: 91 percent / 4-DMAP, Et₃N / CH₂Cl₂ / 1 h / 0 °C

2: 81 percent / BF₃*Et₂O, TMSOTf / acetonitrile / 3 h / 0 °C

3: 100 percent / MeONa / methanol / 24 h / 25 °C

4: 1.) n-Bu₂SnO, 2.) CsF / 1.) MeOH, reflux, 4 h, 2.) DMF, 40 deg C, 16 h

5: 1.) imidazole, NaH

6: 60 percent / n-Bu₃SnH, AIBN / toluene / 1 h / 110 °C

7: 1.) O₃, 2.) NaBH₄ / 1.) CH₂Cl₂, MeOH, -78 deg C, 20 min, 2.) CH₂Cl₂, MeOH, from -78 deg C to RT, 7 h

8: 83 percent / Ph₃P, I₂, imidazole / CH₂Cl₂ / 2 h / 40 °C

9: 1.) LDA / 1.) Et₂O, hexane, 0 deg C, 4 h, 2.) Et₂O, hexane, from -110 deg C to RT, 12 h

10: 97 percent / O₃ / CH₂Cl₂ / -78 °C

11: 1.) TiCl₄, Et₃N / 1.) CH₂Cl₂, -78 deg C, 2.5 h, 2.) CH₂Cl₂, -78 deg C, 2.5 h

12: 89 percent / SmI₂ / tetrahydrofuran / 1 h / -10 °C

13: 86 percent / 2,6-lutidine / CH₂Cl₂ / 1 h / 0 - 20 °C

14: 99 percent / H₂ / 10percent Pd/C / ethanol / 48 h / Ambient temperature

15: Et₃N, SOCl₂ / CH₂Cl₂ / 0.17 h / 0 °C

16: RuCl₃, NaIO₄ / CCl₄; acetonitrile; H₂O / 1.5 h / 0 °C

17: 1.) t-BuLi, HMPA, 3.) 30percent aq. H₂SO₄

18: 91 percent / NBS, AgClO₄ / acetone; H₂O / 0.01 h / 0 °C

With 1H-imidazole; 2,6-dimethylpyridine; N,N,N,N,N,N-hexamethylphosphoric triamide; dmap; ruthenium trichloride; sodium tetrahydroborate; sodium periodate; N-Bromosuccinimide; thionyl chloride; samarium diiodide; 2,2'-azobis(isobutyronitrile); trimethylsilyl trifluoromethanesulfonate; sulfuric acid; boron trifluoride diethyl etherate; hydrogen; iodine; tert.-butyl lithium; tri-n-butyl-tin hydride; sodium methylate; silver perchlorate; titanium tetrachloride; sodium hydride; di(n-butyl)tin oxide; ozone; triethylamine; triphenylphosphine; cesium fluoride; lithium diisopropyl amide; palladium on activated charcoal; In tetrahydrofuran; methanol; tetrachloromethane; ethanol; dichloromethane; water; acetone; toluene; acetonitrile;