naphthalen-2-yl (S)-2-((4-methoxyphenyl)(4-methoxyphenylsulfonamido)methyl)-acrylate

Base Information

Chemical Name:naphthalen-2-yl (S)-2-((4-methoxyphenyl)(4-methoxyphenylsulfonamido)methyl)-acrylate
CAS No.:1056904-16-5
Molecular Formula:C₂₈H₂₅NO₆S
Molecular Weight:503.576
Hs Code.:

Synonyms:naphthalen-2-yl (S)-2-((4-methoxyphenyl)(4-methoxyphenylsulfonamido)methyl)-acrylate

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Chemical Property of naphthalen-2-yl (S)-2-((4-methoxyphenyl)(4-methoxyphenylsulfonamido)methyl)-acrylate

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Technology Process of naphthalen-2-yl (S)-2-((4-methoxyphenyl)(4-methoxyphenylsulfonamido)methyl)-acrylate

There total 2 articles about naphthalen-2-yl (S)-2-((4-methoxyphenyl)(4-methoxyphenylsulfonamido)methyl)-acrylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 52684-34-1
2-naphthyl acrylate

: 73845-03-1
4-Methoxy-N-[1-(4-methoxy-phenyl)-meth-(E)-ylidene]-benzenesulfonamide

: 1056904-16-5
naphthalen-2-yl (S)-2-((4-methoxyphenyl)(4-methoxyphenylsulfonamido)methyl)-acrylate

Guidance literature:: With 6'-N-boc-glycine-β-ICD; β-naphthol; In dichloromethane; at -30 ℃; for 80h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1021/ja805122j

Reference yield:

: 52684-34-1
2-naphthyl acrylate

: 73845-03-1
4-Methoxy-N-[1-(4-methoxy-phenyl)-meth-(E)-ylidene]-benzenesulfonamide

: 1056904-16-5
naphthalen-2-yl (S)-2-((4-methoxyphenyl)(4-methoxyphenylsulfonamido)methyl)-acrylate

: naphthalen-2-yl (R)-2-((4-methoxyphenyl)(4-methoxyphenylsulfonamido)methyl)-acrylate

Guidance literature:: With tert-butyl (2-((4-((1R)-7-ethylhexahydro-1H-3,7-methanopyrrolo[2,1-c][1,4]oxazin-1-yl)quinolin-6-yl)amino)-2-oxoethyl)carbamate; β-naphthol; In dichloromethane; at -30 ℃; for 72h; Overall yield = 80 %; enantioselective reaction; Inert atmosphere;
DOI:10.1002/chem.201302665