ethyl N-{(3,5-dibromobiphenyl-4-yl)[3,5-bis(trifluoromethyl)biphenyl-4-yl]methyl}carbamate

Base Information

Chemical Name:ethyl N-{(3,5-dibromobiphenyl-4-yl)[3,5-bis(trifluoromethyl)biphenyl-4-yl]methyl}carbamate
CAS No.:876758-58-6
Molecular Formula:C₃₀H₂₁Br₂F₆NO₂
Molecular Weight:701.301
Hs Code.:

Synonyms:ethyl N-{(3,5-dibromobiphenyl-4-yl)[3,5-bis(trifluoromethyl)biphenyl-4-yl]methyl}carbamate

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Chemical Property of ethyl N-{(3,5-dibromobiphenyl-4-yl)[3,5-bis(trifluoromethyl)biphenyl-4-yl]methyl}carbamate

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Technology Process of ethyl N-{(3,5-dibromobiphenyl-4-yl)[3,5-bis(trifluoromethyl)biphenyl-4-yl]methyl}carbamate

There total 5 articles about ethyl N-{(3,5-dibromobiphenyl-4-yl)[3,5-bis(trifluoromethyl)biphenyl-4-yl]methyl}carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 876758-55-3
(3,5-dibromobiphenyl-4-yl)[3,5-bis(trifluoromethyl)biphenyl]chloromethane

: 51-79-6
urethane

: 876758-58-6
ethyl N-{(3,5-dibromobiphenyl-4-yl)[3,5-bis(trifluoromethyl)biphenyl-4-yl]methyl}carbamate

Guidance literature:: urethane; With silver tetrafluoroborate; at 60 ℃;

(3,5-dibromobiphenyl-4-yl)[3,5-bis(trifluoromethyl)biphenyl]chloromethane; In 1,4-dioxane; at 100 ℃;
DOI:10.1021/ja056575j

Reference yield:

: 876758-56-4
3,5-dibromobiphenyl-4-carbaldehyde

: 876758-58-6
ethyl N-{(3,5-dibromobiphenyl-4-yl)[3,5-bis(trifluoromethyl)biphenyl-4-yl]methyl}carbamate

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-BuLi; TMEDA / diethyl ether; hexane / 2 h / Heating

1.2: 46 percent / diethyl ether; hexane; tetrahydrofuran / 4 h / Heating

2.1: SOCl₂ / 20 °C

3.1: AgBF₄ / 60 °C

3.2: 51 mg / dioxane / 100 °C

With silver tetrafluoroborate; n-butyllithium; thionyl chloride; N,N,N,N,-tetramethylethylenediamine; In diethyl ether; hexane;
DOI:10.1021/ja056575j

Reference yield:

: 918415-66-4
3,5-dibromo-4-cyano-1,1'-biphenyl

: 876758-58-6
ethyl N-{(3,5-dibromobiphenyl-4-yl)[3,5-bis(trifluoromethyl)biphenyl-4-yl]methyl}carbamate

Guidance literature:: Multi-step reaction with 4 steps

1.1: DIBAL-H / hexane; CH₂Cl₂ / 0.5 h / 20 °C

1.2: 88 percent / aq. HCl / hexane; CH₂Cl₂ / 1 h / 40 °C

2.1: n-BuLi; TMEDA / diethyl ether; hexane / 2 h / Heating

2.2: 46 percent / diethyl ether; hexane; tetrahydrofuran / 4 h / Heating

3.1: SOCl₂ / 20 °C

4.1: AgBF₄ / 60 °C

4.2: 51 mg / dioxane / 100 °C

With silver tetrafluoroborate; n-butyllithium; thionyl chloride; N,N,N,N,-tetramethylethylenediamine; diisobutylaluminium hydride; In diethyl ether; hexane; dichloromethane;
DOI:10.1021/ja056575j