3-<2-<3-<5-(benzyloxy)-2-ethyl-4-(4-fluorophenyl)phenoxy>propoxy>-6-methoxyphenyl>propanoic acid ethyl ester

Base Information

Chemical Name:3-<2-<3-<5-(benzyloxy)-2-ethyl-4-(4-fluorophenyl)phenoxy>propoxy>-6-methoxyphenyl>propanoic acid ethyl ester
CAS No.:152608-90-7
Molecular Formula:C₃₆H₃₉FO₆
Molecular Weight:586.7
Hs Code.:

Synonyms:3-<2-<3-<5-(benzyloxy)-2-ethyl-4-(4-fluorophenyl)phenoxy>propoxy>-6-methoxyphenyl>propanoic acid ethyl ester

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Chemical Property of 3-<2-<3-<5-(benzyloxy)-2-ethyl-4-(4-fluorophenyl)phenoxy>propoxy>-6-methoxyphenyl>propanoic acid ethyl ester

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Technology Process of 3-<2-<3-<5-(benzyloxy)-2-ethyl-4-(4-fluorophenyl)phenoxy>propoxy>-6-methoxyphenyl>propanoic acid ethyl ester

There total 8 articles about 3-<2-<3-<5-(benzyloxy)-2-ethyl-4-(4-fluorophenyl)phenoxy>propoxy>-6-methoxyphenyl>propanoic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 152120-07-5
2-benzyloxy-1-(4-fluorophenyl)-5-ethyl-4-(3-chloro-1-propyloxy)benzene

: 152608-83-8
ethyl 3-(2-hydroxy-6-methoxyphenyl)propionate

: 152608-90-7
3-<2-<3-<5-(benzyloxy)-2-ethyl-4-(4-fluorophenyl)phenoxy>propoxy>-6-methoxyphenyl>propanoic acid ethyl ester

Guidance literature:: With potassium carbonate; dimethyl sulfoxide; potassium iodide; In butanone; for 18h; Heating;
DOI:10.1021/jm00022a006

Reference yield:

: 150-19-6
O-methylresorcine

: 152608-90-7
3-<2-<3-<5-(benzyloxy)-2-ethyl-4-(4-fluorophenyl)phenoxy>propoxy>-6-methoxyphenyl>propanoic acid ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: pivalic acid / toluene / 16 h / Heating

2: 1 N HCl / tetrahydrofuran / 1 h

3: 44 percent / K₂CO₃, KI, DMSO / butan-2-one / 18 h / Heating

With hydrogenchloride; potassium carbonate; dimethyl sulfoxide; potassium iodide; Trimethylacetic acid; In tetrahydrofuran; toluene; butanone;
DOI:10.1021/jm00022a006

Reference yield:

: 29682-12-0
1-[4-(benzyloxy)-2-hydroxyphenyl]ethanone

: 152608-90-7
3-<2-<3-<5-(benzyloxy)-2-ethyl-4-(4-fluorophenyl)phenoxy>propoxy>-6-methoxyphenyl>propanoic acid ethyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 82 percent / K₂CO₃ / dimethylsulfoxide; butan-2-one / 24 h / Heating

2: 69 percent / trifluoroacetic acid, triethylsilane / CCl₄ / 1.5 h / Ambient temperature

3: 73 percent / N-bromosuccinimide / CCl₄ / 6 h / Ambient temperature

4: 84 percent / Pd(PPh₃)4, aq. Na₂CO₃ / ethanol; benzene / 16 h / Heating

5: 44 percent / K₂CO₃, KI, DMSO / butan-2-one / 18 h / Heating

With triethylsilane; N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; potassium carbonate; dimethyl sulfoxide; trifluoroacetic acid; potassium iodide; In tetrachloromethane; ethanol; dimethyl sulfoxide; butanone; benzene;
DOI:10.1021/jm00022a006