Technology Process of 2-methoxy-4-n-pentylbenzylaldehyde
There total 6 articles about 2-methoxy-4-n-pentylbenzylaldehyde which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
pyridinium chlorochromate;
In
dichloromethane;
for 0.25h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 85 percent / potassium carbonate / acetone / 12 h / Heating
2: 79.3 percent / NaOBr / H2O; bis-(2-methoxy-ethyl) ether / 30 - 40 °C
3: 85.5 percent / LAH / diethyl ether
4: 97.5 percent / pyridinium chlorochromate / CH2Cl2 / 0.25 h
With
lithium aluminium tetrahydride; sodium hypobromide; potassium carbonate; pyridinium chlorochromate;
In
diethyl ether; dichloromethane; diethylene glycol dimethyl ether; water; acetone;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 95 percent / pyridine / 4 h
2: 62.5 percent / aluminium chloride / 2.5 h / 165 °C
3: 85 percent / potassium carbonate / acetone / 12 h / Heating
4: 79.3 percent / NaOBr / H2O; bis-(2-methoxy-ethyl) ether / 30 - 40 °C
5: 85.5 percent / LAH / diethyl ether
6: 97.5 percent / pyridinium chlorochromate / CH2Cl2 / 0.25 h
With
pyridine; lithium aluminium tetrahydride; aluminium trichloride; sodium hypobromide; potassium carbonate; pyridinium chlorochromate;
In
diethyl ether; dichloromethane; diethylene glycol dimethyl ether; water; acetone;
