(1R,2S,3S,4S)-1,2,3,4,5-pentahydroxy-7-methoxy-2-methyl-1,2,3,4-tetrahydroanthracene-9,10-dione

Base Information

Chemical Name:(1R,2S,3S,4S)-1,2,3,4,5-pentahydroxy-7-methoxy-2-methyl-1,2,3,4-tetrahydroanthracene-9,10-dione
CAS No.:149715-93-5
Molecular Formula:C₁₆H₁₆O₈
Molecular Weight:336.298
Hs Code.:
Mol file:149715-93-5.mol

Synonyms:9,10-Anthracenedione,1,2,3,4-tetrahydro-1,2,3,4,5-pentahydroxy-7-methoxy-2-methyl-, [1R-(1a,2b,3a,4a)]-; Altersolanol E

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Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1R,2S,3S,4S)-1,2,3,4,5-pentahydroxy-7-methoxy-2-methyl-1,2,3,4-tetrahydroanthracene-9,10-dione

Chemical Property:

Vapor Pressure:3.77E-18mmHg at 25°C
Boiling Point:656.9°C at 760 mmHg
Flash Point:246.5°C
Density:1.7g/cm³

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of (1R,2S,3S,4S)-1,2,3,4,5-pentahydroxy-7-methoxy-2-methyl-1,2,3,4-tetrahydroanthracene-9,10-dione

There total 15 articles about (1R,2S,3S,4S)-1,2,3,4,5-pentahydroxy-7-methoxy-2-methyl-1,2,3,4-tetrahydroanthracene-9,10-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: (1aR,2R,3S,9bS)-3-((tert-butyldimethylsilyl)oxy)-2,5-dihydroxy-7-methoxy-1a-methyl-1a,2,3,9b-tetrahydroanthra[1,2-b]oxirene-4,9-dione

: 116948-40-4,116948-41-5,149715-93-5,22268-16-2,31179-82-5,55809-88-6
altersolanol A

Guidance literature:: With sulfuric acid; In tetrahydrofuran; water; at 20 ℃; for 72h; Schlenk technique; Inert atmosphere;
DOI:10.1039/c8ob02113a

Reference yield: 49.0%

: 116889-06-6
(1RS,2RS,3SR,4SR)-3,4-epoxy-1,2,3,4-tetrahydro-2,5-dihydroxy-7-methoxy-2-methyl-1-(trimethylsiloxy)-9,10-anthraquinone

: 22268-16-2,116948-40-4,116948-41-5,149715-93-5,31179-82-5,55809-88-6
(1RS,2SR,3SR,4RS)-1,2,3,4-tetrahydro-1,2,3,4,5-pentahydroxy-7-methoxy-2-methyl-9,10-anthraquinone

Guidance literature:: With sulfuric acid; In tetrahydrofuran; water; for 72h; Ambient temperature;

Reference yield:

: (+)-aS-alterporriol C

: 14717-90-9
6-O-methylalaternin

: 22225-67-8
macrosporin

: 116948-40-4,116948-41-5,149715-93-5,22268-16-2,31179-82-5,55809-88-6
altersolanol A

Guidance literature:: With sodium hydroxide; sodium dithionite; In water; at 70 ℃; for 0.5h; Product distribution; determination TLC;
DOI:10.1016/0031-9422(88)80036-0