methyl 4-(benzyloxy)butanoylcarbamate

Base Information

Chemical Name:methyl 4-(benzyloxy)butanoylcarbamate
CAS No.:1416151-34-2
Molecular Formula:C₁₃H₁₇NO₄
Molecular Weight:251.282
Hs Code.:

Synonyms:methyl 4-(benzyloxy)butanoylcarbamate

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Chemical Property of methyl 4-(benzyloxy)butanoylcarbamate

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Technology Process of methyl 4-(benzyloxy)butanoylcarbamate

There total 2 articles about methyl 4-(benzyloxy)butanoylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1416151-32-0
C₁₄H₁₉NO₄

: 1416151-34-2
methyl 4-(benzyloxy)butanoylcarbamate

Guidance literature:: With pyridinium p-toluenesulfonate; In tetrahydrofuran; water; at 20 ℃; for 12h; Inert atmosphere;
DOI:10.1021/ol303062a

Reference yield:

: 14593-43-2
benzyl allyl ether

: 1416151-34-2
methyl 4-(benzyloxy)butanoylcarbamate

Guidance literature:: Multi-step reaction with 3 steps

1: tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; copper(I) thiophene-2-carboxylate; caesium carbonate / tetrahydrofuran / 6 h / 50 °C / Inert atmosphere

3: pyridinium p-toluenesulfonate / tetrahydrofuran; water / 12 h / 20 °C / Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; copper(I) thiophene-2-carboxylate; pyridinium p-toluenesulfonate; caesium carbonate; In tetrahydrofuran; water;
DOI:10.1021/ol303062a