4-((3-((dimethylamino)methyl)-2-methyl-1H-indol-1-yl)methyl)-N-hydroxybenzamide

Base Information

Chemical Name:4-((3-((dimethylamino)methyl)-2-methyl-1H-indol-1-yl)methyl)-N-hydroxybenzamide
CAS No.:1392835-46-9
Molecular Formula:C₂₀H₂₃N₃O₂
Molecular Weight:337.422
Hs Code.:

Synonyms:4-((3-((dimethylamino)methyl)-2-methyl-1H-indol-1-yl)methyl)-N-hydroxybenzamide

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Chemical Property of 4-((3-((dimethylamino)methyl)-2-methyl-1H-indol-1-yl)methyl)-N-hydroxybenzamide

Chemical Property:

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Technology Process of 4-((3-((dimethylamino)methyl)-2-methyl-1H-indol-1-yl)methyl)-N-hydroxybenzamide

There total 5 articles about 4-((3-((dimethylamino)methyl)-2-methyl-1H-indol-1-yl)methyl)-N-hydroxybenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1392835-46-9
4-((3-((dimethylamino)methyl)-2-methyl-1H-indol-1-yl)methyl)-N-hydroxybenzamide

Guidance literature:

Reference yield:

: C₂₇H₂₉N₃O₂

: 1392835-46-9
4-((3-((dimethylamino)methyl)-2-methyl-1H-indol-1-yl)methyl)-N-hydroxybenzamide

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In methanol; at 20 ℃; for 6h;
DOI:10.1016/j.ejmech.2016.12.039

Reference yield:

: 4-((3-formyl-2-methyl-1H-indol-1-yl)methyl)benzoic acid

: 1392835-46-9
4-((3-((dimethylamino)methyl)-2-methyl-1H-indol-1-yl)methyl)-N-hydroxybenzamide

Guidance literature:: Multi-step reaction with 3 steps

1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 °C

2: sodium tris(acetoxy)borohydride / dichloromethane / 20 °C

3: palladium 10% on activated carbon; hydrogen / methanol / 6 h / 20 °C

With palladium 10% on activated carbon; hydrogen; sodium tris(acetoxy)borohydride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2016.12.039