(S)-benzyl 1-[1-(ethoxymethyl)-2-iodo-1H-imidazol-4-yl]-3-methylbutylcarbamate

Base Information

Chemical Name:(S)-benzyl 1-[1-(ethoxymethyl)-2-iodo-1H-imidazol-4-yl]-3-methylbutylcarbamate
CAS No.:1135467-17-2
Molecular Formula:C₁₉H₂₆IN₃O₃
Molecular Weight:471.338
Hs Code.:

Synonyms:(S)-benzyl 1-[1-(ethoxymethyl)-2-iodo-1H-imidazol-4-yl]-3-methylbutylcarbamate

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Chemical Property of (S)-benzyl 1-[1-(ethoxymethyl)-2-iodo-1H-imidazol-4-yl]-3-methylbutylcarbamate

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Technology Process of (S)-benzyl 1-[1-(ethoxymethyl)-2-iodo-1H-imidazol-4-yl]-3-methylbutylcarbamate

There total 1 articles about (S)-benzyl 1-[1-(ethoxymethyl)-2-iodo-1H-imidazol-4-yl]-3-methylbutylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 1135467-14-9
(S)-benzyl 1-[1-(ethoxymethyl)-1H-imidazol-4-yl]-3-methylbutylcarbamate

: 1135467-17-2
(S)-benzyl 1-[1-(ethoxymethyl)-2-iodo-1H-imidazol-4-yl]-3-methylbutylcarbamate

Guidance literature:: (S)-benzyl 1-[1-(ethoxymethyl)-1H-imidazol-4-yl]-3-methylbutylcarbamate; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; Inert atmosphere;

With iodine; In tetrahydrofuran; hexane; at -78 - 25 ℃; for 14h; optical yield given as %ee;
DOI:10.1055/s-0028-1083263

Reference yield: 88.0%

: 13331-23-2
fur-2-ylboronic acid

: 1135467-17-2
(S)-benzyl 1-[1-(ethoxymethyl)-2-iodo-1H-imidazol-4-yl]-3-methylbutylcarbamate

: 1135467-28-5
(S)-benzyl 1-[1-(ethoxymethyl)-2-(furan-2-yl)-1H-imidazol-4-yl]-3-methylbutylcarbamate

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In tetrahydrofuran; water; for 6h; optical yield given as %ee; Reflux;
DOI:10.1055/s-0028-1083263